苯甲基(氯甲基)二甲基硅烷合成路线 (共 4 条)
反应条件
1: 12 h / 80 °C 2: 1.) sec-butyllithium / 1.) THF, 2.) ether 3: 91 percent / H2O2, KF, KHCO3 / 15 h / Ambient temperature View Scheme
参考文献
Chan, T. H.; Pellon, P.
Journal of the American Chemical Society, 1989 , vol. 111, # 23 p. 8737 - 8738
反应条件
iodine; magnesium in tetrahydrofuran
参考文献
Hoechst Marion Roussel, Inc.
Patent: US5608095 A1, 1997 ;
反应条件
in tetrahydrofuran; hexane; nitrogen
参考文献
BioSurface Engineering Technologies, Inc.
Patent: US6342591 B1, 2002 ;
反应条件
in diethyl ether
Heating;
参考文献
Fraenkel, Gideon; Martin, Kevin V.
Journal of the American Chemical Society, 1995 , vol. 117, # 41 p. 10336 - 10344