(S)-3-羟基丁酸甲酯合成路线 (共 36 条)
反应条件
lt;Ru((S)-(-)-BINAPgt; cat; hydrogen in methanol; dichloromethane T=25°C; P=77572.2 Torr; 48 h;
参考文献
Enev; Harre; Nickisch; Schneider; Mohr
Tetrahedron Asymmetry, 2000 , vol. 11, # 8 p. 1767 - 1779
反应条件
Ru2Cl4-(S)-(2,2'-bis(diphenylphosphino)-1,1'-binaphthyl)2*NEt3; hydrogen in methanol T=35°C; P=76000.1 Torr; 48 h; Title compound not separated from byproducts;
参考文献
Shao, Liming; Takeuchi, Kasumi; Ikemoto, Makoto; Kawai, Toshiyasu; Ogasawara, Masamichi; et al.
Journal of Organometallic Chemistry, 1992 , vol. 435, # 1.2 p. 133 - 147
反应条件
hydrogen; [Ru(p-cymene)I-(S)-binap]I in methanol T=30°C; P=76000 Torr; 35 h;
参考文献
Journal of Organic Chemistry, , vol. 59, # 11 p. 3064 - 3076
反应条件
sodium peroxoborate tetrahydrate in tetrahydrofuran; water T=20°C; 1 h;
参考文献
Tetrahedron Asymmetry, , vol. 23, # 17 p. 1294 - 1300
反应条件
hydrogen; [Ru(p-cymene)I-(S)-binap]I in methanol T=30°C; P=76000 Torr; 35 h; other: catalysts, solvents, time, pressure, temperatures; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 59, # 11 p. 3064 - 3076
反应条件
dicobalt octacarbonyl T=20°C; P=760.051 Torr; 24 h;
参考文献
Denmark, Scott E.; Ahmad, Moballigh
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9630 - 9634
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol 4 h;
参考文献
Larcheveque; Mambu; Petit
Synthetic Communications, 1991 , vol. 21, # 22 p. 2295 - 2300
参考文献
Lian, Huiling; Whitman, Christian P.
Journal of the American Chemical Society, 1994 , vol. 116, # 23 p. 10403 - 10411
反应条件
NaBO3*H2O in tetrahydrofuran; methanol; water T=20°C; 12 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 7, # 12 p. 2520 - 2524
反应条件
[Ru(R)-Binap(benzene)Cl]Cl; hydrogen in water T=17°C; P=69873.2 Torr; 44 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 17 p. 1208 - 1210