反应条件
1: 1.) Na2SO3, NaHCO3 / 1.) H2O, 10 h, 2.) 1 h
2: Et3N / CH2Cl2 / 1 h / Ambient temperature
3: 1.) Mg / 1.) Et2O, 2.) reflux, 1 h
4: (AcO)2Cu / acetic acid; H2O / 0.67 h / Heating
5: 85percent hydrazine hydrate / butan-1-ol / Heating
6: O2, CuCl / pyridine
7: acetic acid / 10 h / 50 °C
View Scheme
参考文献
Oprean, I.; Ciupe, Hilke; Gansca, Lucia; Hodosan, F.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 2 p. 283 - 289
