1,3,5-三氮杂-7-磷代金刚烷合成路线 (共 10 条)
反应条件
in water; acetone B-complex reacted with water in acetone/water (1:1) at 80°C for ca. 48 h; detn. by IR, 11B-NMR;
参考文献
Bolano, Sandra; Albinati, Alberto; Bravo, Jorge; Gonsalvi, Luca; Peruzzini, Maurizio
Inorganic Chemistry Communications, 2006 , vol. 9, # 4 p. 360 - 363
参考文献
Navech, Jacques; Kraemer, Raymond; Majoral, Jean-Pierre
Tetrahedron Letters, 1980 , vol. 21, p. 1449 - 1452
反应条件
sodium hydroxide; ammonia; hydrazine hydrate in water 1.) 0 deg C, 2.) room temperature, 18 h; Title compound not separated from byproducts;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 14, p. 105 - 120
反应条件
hexamethylene diamine; sodium hydroxide; ammonia in water 1.) 0 deg C, 2.) room temperature, 18 h; Title compound not separated from byproducts;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 14, p. 105 - 120
反应条件
sodium hydroxide; ammonia in water 1.) 0 deg C, 2.) room temperature, 18 h; Title compound not separated from byproducts;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 14, p. 105 - 120
反应条件
KSeCN in methanol
T=20°C; 0.166667 h;
参考文献
Otto, Stefanus; Ionescu, Adriana; Roodt, Andreas
Journal of Organometallic Chemistry, 2005 , vol. 690, # 19 p. 4337 - 4342
反应条件
sulfur in water
0.5 h; Heating;
参考文献
Fisher, Keith J.; Alyea, Elmer C.; Shahnazarian, Noel
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 48, # 1-4 p. 37 - 40
参考文献
Siele,V.I.
Journal of Heterocyclic Chemistry, 1977 , vol. 14, p. 337 - 339
反应条件
dinitrogen tetraoxide in chloroform
参考文献
Benhammou, Malika; Kraemer, Raymond; Germa, Helene; Majoral, Jean-Pierre; Navech, Jacques
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 14, p. 105 - 120
参考文献
Fisher, Keith J.; Alyea, Elmer C.; Shahnazarian, Noel
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 48, # 1-4 p. 37 - 40