2'-溴-4-氯苯乙酮合成路线 （共 272 条）
反应条件
1: 2-[(1,3,2-dioxaborolan-2-yloxy)diphenylmethyl]pyrrolidine; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 2: sodium hydroxide / tetrahydrofuran; water / 2 h View Scheme
参考文献
Huang, Kun; Wang, Haiyang; Stepanenko, Viatcheslav; De Jesus, Melvin; Torruellas, Carilyn; Correa, Wildeliz; Ortiz-Marciales, Margarita
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1883 - 1886
反应条件
NAF in methanol; water T=20°C; 0.0166667 h; Reagent/catalystSolvent;
参考文献
Banothu, Janardhan; Vaarla, Krishnaiah; Bavantula, Rajitha; Crooks, Peter A.
Chinese Chemical Letters, 2014 , vol. 25, # 1 p. 172 - 175
反应条件
aluminum oxide; ammonium acetate; silica gel in benzene T=90°C; 16 h;
参考文献
Jung, Kwan-Young; Kim, Soo-Kyung; Gao, Zhan-Guo; Gross, Ariel S.; Melman, Neli; Jacobson, Kenneth A.; Kim, Yong-Chul
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 3 p. 613 - 623
反应条件
in ethanol; water T=20 - 80°C; 4.167 h;
参考文献
Takeda Chemical Industries, Ltd.; Kusaka, Masami
Patent: EP1348706 A1, 2003 ;
Location in patent: Page/Page column 40 ;
参考文献
Bariana et al.
J.Indian cehm.Soc., 1954 , vol. 31, p. 848,851
反应条件
in dichloromethane T=20°C;
参考文献
Bhalerao, Dinesh S.; Akamanchi, Krishnacharya G.
Synthetic Communications, 2010 , vol. 40, # 6 p. 799 - 807
反应条件
in ethanol 1 h; Reflux;
参考文献
Baek, Seung-Hwa; Kim, Nakjeong; Kim, Seong Hwan; Park, Kwang Hwa; Jeong, Kyung-Chae; Park, Bae Keun; Kang, Nam Sook
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 1 p. 111 - 114
反应条件
in ethanol 6 h; Heating;
参考文献
Singh, S. P.; Sehgal, Subhash; Singh, Lukhvinder; Dhawan, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 154 - 155
反应条件
in ethanol 3 h; Heating;
参考文献
Singh; Sehgal; Sing Tarar; Dhawan
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 4 p. 310 - 314
反应条件
triethylamine in ethanol 1 h; Heating;
参考文献
Elnagdi, M. H.; Abdallah, S. O.; Ghoneim, K. M.; Ebied, E. M.; Kassab, K. N.
Journal of Chemical Research, Miniprint, 1997 , # 2 p. 375 - 384
