2'-溴-4-氯苯乙酮合成路线 （共 272 条）
反应条件
carbon tetrabromide; hydrogen bromide; oxygen in dichloromethane; water 10 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 52, # 29 p. 3821 - 3824
反应条件
tetrasulphur tetranitride T=115°C; 10 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 3 p. 253 - 260
反应条件
hydrogen cation in water T=25°C; Rate constant;
参考文献
Bulletin de la Societe Chimique de France, , # 2 p. 313 - 316
反应条件
aluminium trichloride
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 125, p. 718
反应条件
water; hydrogen bromide; oxygen 20 h; Irradiation;
参考文献
Synlett, , # 10 art. no. U01411ST, p. 1381 - 1384
反应条件
20 h; Inert atmosphereIrradiation;
参考文献
Synlett, , # 10 art. no. U01411ST, p. 1381 - 1384
反应条件
1: NaH / tetrahydrofuran / 0.5 h / Ambient temperature 2: acetic anhydride / 0.25 h / 40 °C View Scheme
参考文献
Ogata, Masaru; Matsumoto, Hiroshi; Kida, Shiro; Shimizu, Sumio; Tawara, Katsuya; Kawamura, Yoshimi
Journal of Medicinal Chemistry, 1987 , vol. 30, # 8 p. 1497 - 1502
反应条件
1: 1.2 g / KOH / dimethylformamide / 0.5 h / Ambient temperature 2: acetic anhydride / 0.25 h / 40 °C View Scheme
参考文献
Ogata, Masaru; Matsumoto, Hiroshi; Kida, Shiro; Shimizu, Sumio; Tawara, Katsuya; Kawamura, Yoshimi
Journal of Medicinal Chemistry, 1987 , vol. 30, # 8 p. 1497 - 1502
反应条件
1: 1.2 g / KOH / dimethylformamide / 0.5 h / Ambient temperature 2: 73 percent / AcOH, piperidine / toluene / 2 h / Heating View Scheme
参考文献
Ogata, Masaru; Matsumoto, Hiroshi; Kida, Shiro; Shimizu, Sumio; Tawara, Katsuya; Kawamura, Yoshimi
Journal of Medicinal Chemistry, 1987 , vol. 30, # 8 p. 1497 - 1502
反应条件
1: 1.) sodium pellets / 1.) toluene, room temp., 3 days, 2.) toluene, 0 deg C, 1 h then room temp., 1 day 2: 49 percent / 12 M hydrochloric acid / ethanol / 24 h / Heating 3: 55 percent / lithium aluminum hydride / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Porretta; Scalzo; Chimenti; Bolasco; Biava; Fischetti; Riccardi
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 5 p. 629 - 639
