2'-溴-4-氯苯乙酮合成路线 （共 272 条）
反应条件
T=30°C; 4 h; Ionic liquid;
参考文献
Kumar, Anil; Muthyala, Manoj Kumar
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5368 - 5370
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C
2: toluene-4-sulfonic acid / benzene / |Dean-Stark
3: dihydrogen peroxide / acetic acid / |Heating
View Scheme
参考文献
Savka; Pohodylo; Obushak
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, 2014 , vol. 50, # 2 p. 303 - 304,2
反应条件
1: ethanol / Heating
2: TsN3, Et3N / ethanol
3: aq. HClO4, Cu
View Scheme
参考文献
Ferdinand,G. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1713 - 1726
反应条件
1: ethanol / Heating
2: TsN3, Et3N / ethanol
3: aq. HClO4, Cu
View Scheme
参考文献
Ferdinand,G. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1713 - 1726
反应条件
1: [3,4-a]phthalazine; 2-bromo-1-(4-chloro-phenyl)-ethanone With (+/-)-2-Ethyloxirane
0.5 h;
2: dimethyl acetylenedicarboxylate With (+/-)-2-Ethyloxirane
12 h; Reflux;
参考文献
Dumitrascu, Florea; Caproiu, Miron Teodor; Georgescu, Florentina; Draghici, Bogdan; Popa, Marcel Mirel; Georgescu, Emilian
Synlett, 2010 , # 16 p. 2407 - 2410
反应条件
potassium carbonate in methanol
pH=11; 0.05 h; microwave irradiation;
参考文献
Kidwai; Venkataramanan; Dave
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 5 p. 1045 - 1047
反应条件
in methanol
0.333333 h; Heating;
参考文献
Kolos, N. N.; Orlov, V. D.; Slobodina, E. K.; Yur'eva, E. Yu.; Korshunov, S. P.; Tue, Zyong van
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 2 p. 222 - 227
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 2 p. 267 - 272
参考文献
Bahner et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3499
反应条件
1: diethyl ether
2: aluminium isopropylate; isopropyl alcohol
View Scheme
参考文献
Lutz et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 617,680
参考文献
Bahner et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3499
