1-(4-甲基苯基)-1-乙醇合成路线 （共 146 条）
反应条件
Sodium bromate; sulfuric acid; sodium bromide in water T=60°C; 0.05 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 51, # 51 p. 6695 - 6699
反应条件
in acetone T=25°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 35, # 47 p. 8751 - 8754
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C 2: iodine / neat (no solvent) / 2 h / 85 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 12 p. 1978 - 1999
反应条件
1: tributylphosphine / toluene / 20 h / 20 °C 2: Thermobifida fusca recombinant phenylacetone monooxygenase; phosphite dehydrogenase; NADPH; sodium phosphite / dimethyl sulfoxide / 8 h / 30 °C / pH 7.5 / |Enzymatic reaction View Scheme
参考文献
Tetrahedron, , vol. 68, # 51 p. 10431 - 10436,6
Tetrahedron, , vol. 68, # 51 p. 10431 - 10436
反应条件
potassium peroxodisulfate bei der Destillation;
参考文献
Chemische Berichte, , vol. 57, p. 1819
反应条件
T=200 - 210°C; P=100 Torr;
参考文献
Journal of Organic Chemistry, , vol. 13, p. 303,305, 306
反应条件
palladium dichloride in methanol T=40°C; 12 h; Inert atmosphereGreen chemistry; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 2-3 p. 341 - 347
反应条件
ammonia; lithium; sodium hydride 1.) ether, C2H5OH, 18, RT 2.) C2H5OH, 30 min, -40 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Liebigs Annalen der Chemie, , # 7 p. 1248 - 1254
反应条件
1.1: potassium bromide / water / 0.17 h / 25 °C / |Resolution of racemate 1.2: 2 h / 25 °C 2.1: sodium tetrahydroborate 3.1: potassium bromide / water / 0.17 h / 25 °C / |Resolution of racemate 3.2: 2 h / 25 °C View Scheme
参考文献
Tan, Rong; Dong, Yan; Peng, Ming; Zheng, Weiguo; Yin, Donghong
Applied Catalysis A: General, 2013 , vol. 458, p. 1 - 10
反应条件
1.1: potassium bromide / water / 0.17 h / 25 °C / |Resolution of racemate 1.2: 2 h / 25 °C 2.1: sodium tetrahydroborate 3.1: potassium bromide / water / 0.17 h / 25 °C / |Resolution of racemate 3.2: 2 h / 25 °C View Scheme
参考文献
Tan, Rong; Dong, Yan; Peng, Ming; Zheng, Weiguo; Yin, Donghong
Applied Catalysis A: General, 2013 , vol. 458, p. 1 - 10
