1-(4-甲基苯基)-1-乙醇合成路线 （共 146 条）
反应条件
pyridine; silver trifluoromethanesulfonate; trichloromethyl chloroformate
1) ether, 0 deg C, 15 min, 2) r.t., 2 h; Yield given. Multistep reaction;
参考文献
Takeda, Kazuyoshi; Ayabe, Akira; Kawashima, Hideki; Harigaya, Yoshihiro
Tetrahedron Letters, 1992 , vol. 33, # 7 p. 951 - 952
反应条件
1: hydrogen bromide / diethyl ether / 48 h
2: 65 percent / silver nitrite / diethyl ether / 24 h / in dark
View Scheme
参考文献
Fischer, Alfred; Henderson, George N.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2314 - 2327
反应条件
in acetone
T=25°C; 3 h;
参考文献
Kovac, F.; Baumstark, A. L.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8751 - 8754
反应条件
1: PBr3, Py / diethyl ether
2: NaOEt / ethanol
3: (i) aq. KOH, EtOH, (ii) (decarboxylation)
View Scheme
参考文献
Kuchar; Brunova; Rejholec; et al.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, # 2 p. 633 - 646
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C
2: iodine / neat (no solvent) / 2 h / 85 °C
View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
zirconium tetrachloride in acetonitrile
2.5 h; Heating;
参考文献
Das, Biswanath; Krishnaiah, Maddeboina; Veeranjaneyulu, Boyapati; Srinivas, Yallamalla; Rao, Yerra Koteswara
Journal of Chemical Research, 2007 , # 12 p. 717 - 719
