1: phenylacetylene With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; 2: (Z)-diphenyl(β-phenylthiostyryl)selenonium trifluoromethanesulfonate in tetrahydrofuran T=-78°C; 5 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 65, # 26 p. 8893 - 8898
triethylaluminum; sulfur; triphenylphosphine; cobalt(II) 2,4-pentanedionate 1) toluene, -15 to -10 deg C, 5-10 min; 2) toluene, 130 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
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Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 3 p. 339
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