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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯乙炔
合成路线
（共 4628 条）
536-74-3
苯乙炔
→
反应条件
3312-38-7
反应条件
1: CuI, PdCl2(CH3CN)2, PdCl2(PPh3)2 / diethylamine / 72 h / Ambient temperature 2: NaOAc, n-Bu4NCl / Pd(OAc)2 / dimethylformamide / 24 h / 100 °C View Scheme
参考文献
Larock, R. C.; Doty, M. J.; Cacchi, S.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4579 - 4583
50-00-0
甲醛
+
593-51-1
盐酸甲胺
+
536-74-3
苯乙炔
→
反应条件
34706-60-0
1-(甲基氨基)-3-苯基-2-丙炔
反应条件
potassium hydrogencarbonate; copper(l) iodide in water; dimethyl sulfoxide T=30°C; 20 h;
参考文献
Bieber, Lothar W.; Da Silva, Margarete F.
Tetrahedron Letters, 2004 , vol. 45, # 45 p. 8281 - 8283
536-74-3
苯乙炔
→
反应条件
34706-60-0
1-(甲基氨基)-3-苯基-2-丙炔
反应条件
1: 74 percent / ZnCl2 / dioxane / 2.5 h / Heating 2: 82 percent / TEA / CH2Cl2 / 1 h / Ambient temperature 3: 98 percent / NaBH4 / ethanol / Ambient temperature View Scheme
参考文献
Yang, Miao; Odelberg, Shannon J.; Tong, Zongzhong; Li, Dean Y.; Looper, Ryan E.
Tetrahedron, 2013 , vol. 69, # 27-28 p. 5744 - 5750
50-00-0
甲醛
+
536-74-3
苯乙炔
+
74-89-5
甲胺
→
反应条件
34706-60-0
1-(甲基氨基)-3-苯基-2-丙炔
反应条件
暂无反应条件数据
参考文献
Babayan,A.T. et al.
Zhurnal Organicheskoi Khimii, 1973 , vol. 9, p. 467 - 471,472 - 476
→
反应条件
333737-46-5
反应条件
in benzene Pt complex and acetylene at a molar ratio 1:3 were heated under Ar at 65°C for 24 h in a sealed tube; concd.; purified by preparative TLC;
参考文献
Mochida, Kunio; Wada, Tohru; Suzuki, Kaoru; Hatanaka, Wakako; Nishiyama, Yuriko; Nanjo, Masato; Sekine, Akiko; Ohashi, Yuji; Sakamoto, Masato; Yamamoto, Akio
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 123 - 137
504-02-9
1,3-环己二酮
+
536-74-3
苯乙炔
→
反应条件
33158-10-0
反应条件
manganese triacetate; acetic acid
参考文献
Alagoz, Oguzhan; Yilmaz, Mehmet; Pekel, A. Tarik
Synthetic Communications, 2006 , vol. 36, # 8 p. 1005 - 1013
1460-08-8
+
536-74-3
苯乙炔
→
反应条件
33158-10-0
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in toluene T=70°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Xia, Likai; Lee, Yong Rok
European Journal of Organic Chemistry, 2014 , vol. 2014, # 16 p. 3430 - 3442
60060-44-8
2-溴-1,3-环己二酮
+
536-74-3
苯乙炔
→
反应条件
33158-10-0
反应条件
disodium hydrogenphosphate; [Ir(phenylpyridine(-1H))2(4,4′-di-tert-butyl-2,2′-bipyridine)](PF6) in ethanol T=20°C; 12 h; Inert atmosphereIrradiation; Catalytic behavior; Reagent/catalystSolvent;
参考文献
Jiang, Heng; Cheng, Yuanzheng; Zhang, Yan; Yu, Shouyun
Organic Letters, 2013 , vol. 15, # 18 p. 4884 - 4887
536-74-3
苯乙炔
→
反应条件
33158-10-0
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine / tetrahydrofuran / 0.67 h / 0 °C / |Inert atmosphere 2: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 3: (Ph3P)AuCl; silver trifluoromethanesulfonate / dichloromethane / 0.08 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
536-74-3
苯乙炔
→
反应条件
1839-72-1
2-苯基-1-苯并呋喃
+
33158-10-0
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine / tetrahydrofuran / 0.67 h / 0 °C / |Inert atmosphere 2: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 3: silver trifluoromethanesulfonate; methanol; {1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl; toluene-4-sulfonic acid / dichloromethane-d2 / 0.17 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
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