反应条件
1.1: tellurium / tetrahydrofuran; hexane / Inert atmosphere 1.2: 4 h / Inert atmosphere; Reflux 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C 2.2: 2.5 h / -78 - 20 °C 2.3: 0.5 h / 20 °C / Darkness; Cooling with ice 3.1: phosphite dehydrogenase; recombinant phenylacetone monooxygenase from Thermobifida fusca, M446G mutant; NADPH / dimethyl sulfoxide / 4 h / 30 °C / Tris/HCl buffer; Enzymatic reaction View Scheme
参考文献
Brondani, Patricia B.; De Gonzalo, Gonzalo; Fraaije, Marco W.; Andrade, Leandro H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2169 - 2173
