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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯乙炔
合成路线
（共 4628 条）
54509-73-8
+
1942-45-6
4-辛炔
+
536-74-3
苯乙炔
→
反应条件
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Xi, Zhenfeng; Hara, Ryuichiro; Takahashi, Tamotsu
Journal of Organic Chemistry, 1995 , vol. 60, # 14 p. 4444 - 4448
536-74-3
苯乙炔
→
反应条件
16492-63-0
反应条件
in 1,2-dichloro-benzene T=180°C; 24 h; Sealed tube; regioselective reaction;
参考文献
Foster, Robert S.; Adams, Harry; Jakobi, Harald; Harrity, Joseph P. A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4049 - 4064
143321-89-5
+
536-74-3
苯乙炔
→
反应条件
143360-89-8
反应条件
copper(l) iodide; N-methylpyrrolidine-2-carboxamide hydrochloride; caesium carbonate in N,N-dimethyl-formamide T=25°C; Sonogashira cross-coupling; 6 h; Inert atmosphere;
参考文献
Jiang, Huimin; Fu, Hua; Qiao, Renzhong; Jiang, Yuyang; Zhao, Yufen
Synthesis, 2008 , # 15 art. no. F06408SS, p. 2417 - 2426
143321-89-5
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
+
143360-89-8
反应条件
potassium phosphate; Cu[(phen)(PPh3)2]NO2 in 1,4-dioxane T=110°C; 24 h;
参考文献
Slough, Greg A.; Krchnak, Viktor; Helquist, Paul; Canham, Stephen M.
Organic Letters, 2004 , vol. 6, # 17 p. 2909 - 2912
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
143360-89-8
反应条件
DiPPF; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 23 h; Inert atmosphereSealed tube;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
536-74-3
苯乙炔
→
反应条件
143360-89-8
反应条件
1: CuI; triethylamine / Pd(Ph3P)2Cl2 / 20 °C 2: pyridine / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Pace, Paola
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 1001 - 1011
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
+
143360-89-8
反应条件
bis(benzonitrile)palladium(II) dichloride; potassium acetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 1.2 h; Inert atmosphereSealed tube; regiospecific reaction;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
108-86-1
溴代苯
+
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
+
3469-20-3
2,3-二苯基吲哚
+
143360-89-8
反应条件
1: 2-bromo-N-(trifluoroacetyl)aniline; phenylacetylene With bis(benzonitrile)palladium(II) dichloride; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 5 h; Inert atmosphereSealed tube; 2: bromobenzene in N,N-dimethyl-formamide T=80°C; 8 h; Inert atmosphereSealed tube; regiospecific reaction;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
108-86-1
溴代苯
+
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
3469-20-3
2,3-二苯基吲哚
+
143360-89-8
反应条件
1: 2-bromo-N-(trifluoroacetyl)aniline; phenylacetylene With palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in N,N-dimethyl-formamide T=80°C; Sonogashira Cross-Coupling; 1.5 h; Inert atmosphereSealed tube; 2: bromobenzene in N,N-dimethyl-formamide T=80°C; 2 h; Inert atmosphereSealed tube; Reagent/catalystTime; regiospecific reaction;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
108-86-1
溴代苯
+
2727-71-1
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
+
143360-89-8
反应条件
1: 2-bromo-N-(trifluoroacetyl)aniline; phenylacetylene With bis(benzonitrile)palladium(II) dichloride; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetonitrile T=80°C; Sonogashira Cross-Coupling; 1.2 h; Inert atmosphereSealed tube; 2: bromobenzene in acetonitrile T=80°C; 2 h; Inert atmosphereSealed tube; regiospecific reaction;
参考文献
Lu, Bruce Z.; Wei, Han-Xun; Zhang, Yongda; Zhao, Wenyi; Dufour, Marine; Li, Guisheng; Farina, Vittorio; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4558 - 4562
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