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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯乙炔
合成路线
（共 4628 条）
536-74-3
苯乙炔
+
189039-67-6
→
反应条件
189039-68-7
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in N,N-dimethyl-formamide T=90°C; 2.5 h;
参考文献
Smith D.W.; Babb; Vernon Snelgrove; Townsend III; Martin
Journal of the American Chemical Society, 1998 , vol. 120, # 35 p. 9078 - 9079
94-67-7
水杨醛肟
+
536-74-3
苯乙炔
→
反应条件
18732-50-8
反应条件
pyridine; N-chloro-succinimide in chloroform 2 h; Heating;
参考文献
Thomsen, Ib; Torssell, Kurt B. G.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 5 p. 303 - 308
3717-21-3
+
536-74-3
苯乙炔
→
反应条件
17064-22-1
反应条件
1: 4-methoxy benzaldehyde oxime With trifluorormethanesulfonic acid; silica gel in toluene T=50°C; 0.5 h; 2: phenylacetylene in toluene T=70°C; 3.5 h; 3: With CuCl2·2H2O; lithium chloride monohydrate; oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane; propan-1-ol; toluene T=60°C; P=9750.98 Torr; 4 h;
参考文献
Yuan, Shizhen; Li, Zhen; Xu, Ling
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 6 p. 1405 - 1409
3532-17-0
+
536-74-3
苯乙炔
→
反应条件
3424-93-9
4-甲氧基苯甲酰胺
+
17064-22-1
反应条件
[Cu(tris(3,5-dimethyl-4-bromopyrazolyl)methane)(MeCN)]BF4 in chloroform T=40°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Cano, Israel; Alvarez, Eleuterio; Nicasio, M. Carmen; Perez, Pedro J.
Journal of the American Chemical Society, 2011 , vol. 133, # 2 p. 191 - 193
3532-17-0
+
536-74-3
苯乙炔
→
反应条件
17064-22-1
反应条件
[(tris(3,5-dimethylpyrazolylmethyl)amine)Cu]PF6 T=40°C; 24 h; Inert atmosphereSchlenk technique;
参考文献
Haldon, Estela; Besora, Maria; Cano, Israel; Cambeiro, Xacobe C.; Pericas, Miquel A.; Maseras, Feliu; Nicasio, M. Carmen; Perez, Pedro J.
Chemistry - A European Journal, 2014 , vol. 20, # 12 p. 3463 - 3474
536-74-3
苯乙炔
+
98-86-2
苯乙酮
→
反应条件
1846-29-3
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C 1.2: 1 h / -78 °C 2.1: 4-methylpyridine 1-oxide; (IPr)AuCl; AgNTf2; bis-(trifluoromethylsulphonyl)amine / dichloromethane / 28 h / 20 °C View Scheme
参考文献
Hashmi, A. Stephen K.; Wang, Tao; Shi, Shuai; Rudolph, Matthias
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7761 - 7767
608-28-6
1,3-二甲基-2-碘苯
+
536-74-3
苯乙炔
→
反应条件
180783-48-6
反应条件
bis-triphenylphosphine-palladium(II) chloride; PPh3 gold(I) chloro complex; triethylamine in N,N-dimethyl-formamide T=80°C; Sonogashira type cross-coupling; 1 h; Inert atmosphere;
参考文献
Panda, Biswajit; Sarkar, Tarunk.
Synthesis (Germany), 2013 , vol. 45, # 6 art. no. SS-2012-Z0931-OP, p. 817 - 829
576-22-7
2-溴-1,3-二甲苯
+
536-74-3
苯乙炔
→
反应条件
180783-48-6
反应条件
dichloro bis(acetonitrile) palladium(II); caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=20°C; Sonogashira coupling; Inert atmosphereMicellar solution;
参考文献
Lipshutz, Bruce H.; Chung, David W.; Rich, Brian
Organic Letters, 2008 , vol. 10, # 17 p. 3793 - 3796
6781-98-2
2-氯-1,3-二甲苯
+
536-74-3
苯乙炔
→
反应条件
180783-48-6
反应条件
dichloro bis(acetonitrile) palladium(II); caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in various solvent(s) T=97°C; Sonogashira coupling; 2.5 h;
参考文献
Gelman, Dmitri; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2003 , vol. 42, # 48 p. 5993 - 5996
→
反应条件
180783-48-6
反应条件
1: phenylacetylene With isopropylmagnesium chloride in tetrahydrofuran T=0 - 20°C; 1 h; Inert atmosphere; 2: (2,6-dimethyl-phenyl)-magnesium iodide With 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in tetrahydrofuran T=66°C; 2.5 h; Inert atmosphere; 3: With water; ammonium chloride in tetrahydrofuran; tert-butyl methyl ether
参考文献
Maji, Modhu Sudan; Murarka, Sandip; Studer, Armido
Organic Letters, 2010 , vol. 12, # 17 p. 3878 - 3881
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