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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯乙炔
合成路线
(共 4628 条)
4001-73-4
2-溴苯甲酰胺
+
536-74-3
苯乙炔
→
反应条件
23023-35-0
3-苯基-1-氨基异喹啉
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 3 h / 120 °C / |Microwave irradiation; |Inert atmosphere 2: ammonium acetate; NaAuCl4*2H2O; silver hexafluoroantimonate / acetonitrile / 20 h / 85 °C View Scheme
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
98262-66-9
+
536-74-3
苯乙炔
→
反应条件
10183-74-1
3-苯基-5,6-二氢-4H-吡咯并[1,2-b]吡唑
+
23894-57-7
反应条件
in xylene 60 h; Heating;
参考文献
Ranganathan, Darshan; Bamezai, Shakti
Synthetic Communications, 1985 , vol. 15, # 3 p. 259 - 266
536-74-3
苯乙炔
+
28123-63-9
Alpha,4-二氯苯甲醛肟
→
反应条件
24097-17-4
3-(4-氯苯基)-5-苯基异恶唑
反应条件
triethylamine in diethyl ether 48 h; Ambient temperature;
参考文献
Bandiera, T.; Gruenanger, P.; Albini, F. Marinone
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 6 p. 1423 - 1428
536-74-3
苯乙炔
+
3848-36-0
4-氯苯甲醛肟
→
反应条件
24097-17-4
3-(4-氯苯基)-5-苯基异恶唑
反应条件
Magtrievetrade; in acetonitrile T=80°C; 2 h;
参考文献
Bhosale, Sandeep; Kurhade, Santosh; Prasad, Uppuleti Viplava; Palle, Venkata P.; Bhuniya, Debnath
Tetrahedron Letters, 2009 , vol. 50, # 27 p. 3948 - 3951
15707-29-6
+
536-74-3
苯乙炔
→
反应条件
2348-81-4
2-氨基-1,4-萘醌
+
1353244-45-7
反应条件
CuSO4‵5H2O; sodium L-ascorbate in water; tert-butyl alcohol T=30°C; 24 h;
参考文献
Do Nascimento, Wilson Silva; Camara, Celso Amorim; De Oliveira, Ronaldo Nascimento
Synthesis, 2011 , # 20 art. no. M54311SS, p. 3220 - 3224
104-94-9
对甲氧基苯胺
+
536-74-3
苯乙炔
→
反应条件
2405-59-6
反应条件
1: With Ti(N(CH3)2)2(C6H5CONC6H3(CH(CH3)2)2)2 in benzene-d6 T=20°C; 24 h; Inert atmosphereSealed tube; 2: With sodium cyanoborohydride; zinc(II) chloride in methanol T=20°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Yim, Jacky C.-H.; Bexrud, Jason A.; Ayinla, Rashidat O.; Leitch, David C.; Schafer, Laurel L.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2015 - 2028
104-94-9
对甲氧基苯胺
+
536-74-3
苯乙炔
→
反应条件
2405-59-6
+
126522-56-3
反应条件
1: With Ti(NMe2)4 in toluene T=80°C; 8 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran; toluene T=80°C; 3 h;
参考文献
Zhou, Fengying; Lin, Miaoshui; Li, Lei; Zhang, Xueqing; Chen, Zhou; Li, Yahong; Zhao, Yang; Wu, Jin; Qian, Guimin; Hu, Bin; Li, Wu
Organometallics, 2011 , vol. 30, # 6 p. 1283 - 1286
536-74-3
苯乙炔
→
反应条件
2491-31-8
反应条件
1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C / |Inert atmosphere 2.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 2 h / 20 °C / |Inert atmosphere 3.1: N-bromosuccinmide / dichloromethane / 3 h / |Inert atmosphere 4.1: sodium hydroxide / N,N-dimethyl-formamide; water / 2 h / 20 °C / |Inert atmosphere 5.1: silver trifluoromethanesulfonate; gold(III) chloride / 1,2-dichloro-ethane / 1 h / 40 °C / |Inert atmosphere 5.2: |Inert atmosphere 5.3: |Inert atmosphere View Scheme
参考文献
Lee, Euichul; Ryu, Taekyu; Park, Youngchul; Park, Sangjune; Lee, Phil Ho
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1585 - 1596
536-74-3
苯乙炔
→
反应条件
4970-78-9
+
114423-86-8
反应条件
water in 1,4-dioxane 6 h; Heating;
参考文献
Tumer, Seniz U.; Herndon, James W.; McMullen, Leonard A.
Journal of the American Chemical Society, 1992 , vol. 114, # 22 p. 8394 - 8404
536-74-3
苯乙炔
→
反应条件
4970-78-9
+
62156-62-1
+
114423-86-8
反应条件
water in 1,4-dioxane 6 h; Heating;
参考文献
Tumer, Seniz U.; Herndon, James W.; McMullen, Leonard A.
Journal of the American Chemical Society, 1992 , vol. 114, # 22 p. 8394 - 8404
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