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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯乙炔
合成路线
（共 4628 条）
589-87-7
对溴碘苯
+
7681-65-4
碘化亚铜
+
536-74-3
苯乙炔
→
反应条件
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
反应条件
triethylamine; bis(triphenylphosphine)palladium(II) chloride in tetrahydrofuran
参考文献
Egawa, Masakazu; Kawakami, Sachiko; Nakashima, Harue; Ohsawa, Nobuharu; Seo, Satoshi; Nomura, Ryoji
Patent: US2007/222374 A1, 2007 ;
536-74-3
苯乙炔
→
反应条件
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C;
参考文献
Grebel-Koehler, Doerthe; Liu, Daojun; De Feyter, Steven; Enkelmann, Volker; Weil, Tanja; Engels, Christiaan; Samyn, Celeste; Muellen, Klaus; De Schryver, Frans C.
Macromolecules, 2003 , vol. 36, # 3 p. 578 - 590
106-37-6
对二溴苯
+
536-74-3
苯乙炔
→
反应条件
1849-27-0
1,4-双(苯乙炔基)苯
+
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
反应条件
tetra-n-butylammonium acetate; [5-Cl-2-{(4-Cl-phenyl)-[(E)-HO-imino]methyl}phenyl-PdCl]2 in 1-methyl-pyrrolidin-2-one T=110°C; Sonogashira coupling; 7.5 h;
参考文献
Alonso, Diego A.; Najera, Carmen; Pacheco, Ma. Carmen
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 9-10 p. 1146 - 1158
589-87-7
对溴碘苯
+
536-74-3
苯乙炔
→
反应条件
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
+
15784-39-1
反应条件
sodium hydroxide; palladium diacetate in water; acetone T=60°C; Sonogashira reaction; 1 h;
参考文献
Shi, Shengyin; Zhang, Yuhong
Synlett, 2007 , # 12 p. 1843 - 1850
65826-67-7
+
536-74-3
苯乙炔
→
反应条件
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
反应条件
triethylamine; AgCl; palladium dichloride in acetonitrile T=20°C; Sonogashira coupling; 0.583333 h;
参考文献
Zhu, Min; Zhou, Zhongshi; Chen, Rui
Synthesis, 2008 , # 17 art. no. P04108SS, p. 2680 - 2682
201230-82-2
+
589-87-7
对溴碘苯
+
536-74-3
苯乙炔
→
反应条件
72758-69-1
+
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
+
93845-79-5
反应条件
copper; zinc; bis(cyclopentadienyl)titanium dichloride; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether T=65°C; 5 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yoshida, Zen-ichi
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3861 - 3864
589-87-7
对溴碘苯
+
536-74-3
苯乙炔
→
反应条件
72758-69-1
+
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
+
93845-79-5
反应条件
carbon monoxide; copper; zinc; bis(cyclopentadienyl)titanium dichloride; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether T=65°C; 5 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yoshida, Zen-ichi
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3861 - 3864
106-37-6
对二溴苯
+
536-74-3
苯乙炔
→
反应条件
1849-27-0
1,4-双(苯乙炔基)苯
+
886-66-8
1,4-二苯基丁二炔
+
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in toluene T=80°C; Sonogashira coupling; 24 h;
参考文献
Chow; Wan; Low; Yeung
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1910 - 1913
673-40-5
4-溴硼酸重氮苯四氟硼酸盐
+
536-74-3
苯乙炔
→
反应条件
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetra-(n-butyl)ammonium iodide; diethylamine in acetonitrile T=20°C; Sonogashira coupling; 2 h; Inert atmosphere;
参考文献
Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio; Cacchi, Sandro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4067 - 4070
536-74-3
苯乙炔
+
106-40-1
对溴苯胺
→
反应条件
13667-12-4
1-(4-溴苯肼)-2-苯乙炔
反应条件
1: 4-bromo-aniline With tert.-butylnitrite; boron trifluoride diethyl etherate in tetrahydrofuran T=-15 - 20°C; Inert atmosphere; 2: phenylacetylene With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetra-(n-butyl)ammonium iodide; diethylamine in acetonitrile T=20°C; Sonogashira coupling; 3 h;
参考文献
Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio; Cacchi, Sandro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4067 - 4070
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