carbon monoxide; palladium on activated charcoal; triphenylphosphine; 1,4-di(diphenylphosphino)-butane in ethylene glycol dimethyl ether T=100°C; P=30400 Torr; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ali, B. El; Vasapollo, G.; Alper, H.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4739 - 4741
carbon monoxide; palladium on activated charcoal; triphenylphosphine; 1,4-di(diphenylphosphino)-butane in ethylene glycol dimethyl ether T=100°C; P=5168 Torr; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ali, B. El; Vasapollo, G.; Alper, H.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4739 - 4741
Reppe
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 1,13, 31
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Reppe,J. W.
Acetylene Chemistry <New York 1949> S. 153, 156