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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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53616-34-5
合成路线
（共 9 条）
53616-34-5
+
75-77-4
三甲基氯硅烷
→
反应条件
89861-14-3
反应条件
n-butyllithium in tetrahydrofuran T=0°C; 2 h;
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
→
反应条件
89861-15-4
反应条件
1: 90 percent / BuLi / tetrahydrofuran / 2 h / 0 °C 2: 99 percent / HCl / methanol / 1 h / Ambient temperature View Scheme
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
+
882-33-7
二苯二硫醚
→
反应条件
89861-16-5
反应条件
n-butyllithium in tetrahydrofuran T=0°C; 12 h;
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
→
反应条件
89861-17-6
反应条件
1: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C 2: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C View Scheme
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
→
反应条件
89861-22-3
反应条件
1: 90 percent / BuLi / tetrahydrofuran / 2 h / 0 °C 2: 99 percent / HCl / methanol / 1 h / Ambient temperature 3: 85 percent / imidazole / dimethylformamide / 12 h / Ambient temperature 4: 92 percent / HOOAc, NaOAc / CH2Cl2 / 3.5 h / 7 °C View Scheme
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
→
反应条件
89861-23-4
反应条件
1: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C 2: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C 3: 95 percent / HCl / methanol / 1 h / Ambient temperature 4: 80 percent / Raney nickel / ethanol / 16 h / Heating 5: 95 percent / imidazole / dimethylformamide / 12 h / Ambient temperature 6: 88 percent / HOOAc, NaOAc / CH2Cl2 / 3.5 h / 7 °C View Scheme
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
→
反应条件
89861-24-5
反应条件
1: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C 2: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C 3: 95 percent / HCl / methanol / 1 h / Ambient temperature 4: 80 percent / Raney nickel / ethanol / 16 h / Heating 5: 80 percent / CBr4, Ph3P View Scheme
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
→
反应条件
89861-25-6
反应条件
1: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C 2: 90 percent / BuLi / tetrahydrofuran / 12 h / 0 °C 3: 95 percent / HCl / methanol / 1 h / Ambient temperature 4: 80 percent / Raney nickel / ethanol / 16 h / Heating 5: 80 percent / CBr4, Ph3P 6: 70 percent / NaH View Scheme
参考文献
Goldsmith, David; Liotta, Dennis; Saindane, Manohar; Waykole, Liladhar; Bowen, Phillip
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5835 - 5838
53616-34-5
→
反应条件
98126-46-6
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane
参考文献
Potvin, Steeves; Canonne, Persephone
Tetrahedron Asymmetry, 1996 , vol. 7, # 10 p. 2821 - 2824
