2-烯丙基-2-甲基丙二酸二乙酯合成路线 （共 8 条）
反应条件
lithium chloride in water; dimethyl sulfoxide 6 h; Heating;
参考文献
Battersby, Alan R.; Westwood, Steven W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1679 - 1688
反应条件
triethylsilane; palladium on activated charcoal in methanol 0.166667 h;
参考文献
Mandal, Pijus K.; McMurray, John S.
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6599 - 6601
反应条件
lithium aluminium tetrahydride in diethyl ether 0.166667 h;
参考文献
Uenishi; Kobayashi; Komine; Okadai; Yonemitsu; Sasaki; Yamada
Chemical and pharmaceutical bulletin, 1999 , vol. 47, # 4 p. 517 - 523
反应条件
1: With NiBr2(PPh3)2; magnesium bromide in tetrahydrofuran; toluene T=20 - 60°C; Inert atmosphere; 2: With ammonium chloride in tetrahydrofuran; water; toluene
参考文献
Organic Letters, , vol. 12, # 10 p. 2254 - 2257
反应条件
titanium(IV) isopropylate; isopropylmagnesium chloride in diethyl ether T=-50 - -40°C; deallylation; 1 h;
参考文献
Yamazaki, Takanori; Urabe, Hirokazu; Sato, Fumie
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 7 p. 1673 - 1681
反应条件
(i) aq. KOH, (ii) (heating); Multistep reaction;
参考文献
Riley,R.G.; Silverstein,R.M.
Tetrahedron, 1974 , vol. 30, p. 1171 - 1174
反应条件
1: With NiBr2(PPh3)2; magnesium bromide in tetrahydrofuran; toluene
T=20 - 60°C; Inert atmosphere;
2: With ammonium chloride in tetrahydrofuran; water; toluene
参考文献
Sumida, Yuto; Yorimitsu, Hideki; Oshima, Koichiro
Organic Letters, 2010 , vol. 12, # 10 p. 2254 - 2257
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium; [(t-Bu3P)PdBr]2 in toluene
T=100°C; P=750.075 Torr; 12 h; Autoclave;
参考文献
Baader, Sabrina; Ohlmann, Dominik M.; Goossen, Lukas J.
Chemistry - A European Journal, 2013 , vol. 19, # 30 p. 9807 - 9810
