反应条件
1: POCl3 / 1.) 25 deg C, 3.5 h, 2.) 50 deg C, 45 min
2: methanol / -5 °C
3: 90 percent / n-BuLi / tetrahydrofuran; hexane / 1.) -65 deg C, 10 min, 2.) -10 deg C, 1 h; 0 deg C, 30 min
4: Na / liquid ammonia; tetrahydrofuran / -50 °C / various reducing agents and medium
View Scheme
参考文献
Veselovskii, V. V.; Novikova, M. A.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 10 p. 2067 - 2070
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 10 p. 2262 - 2266
