3-甲基-4-硝基苯甲醚合成路线 （共 58 条）
参考文献
Bayer Aktiengesellschaft
Patent: US5399773 A1, 1995 ;
反应条件
1: in tetrahydrofuran T=-70°C; 0.0833333 h; 2: With potassium permanganate; ammonia in tetrahydrofuran T=-70°C; 0.25 h;
参考文献
Journal of Organometallic Chemistry, , vol. 624, # 1-2 p. 167 - 171
参考文献
Pavlidis; Perry
Synthetic Communications, 1994 , vol. 24, # 4 p. 533 - 548
反应条件
4-Hydroxy-2-methoxy-6-methylbenzoesaeure-methylester; potassium carbonate; copper(II) oxide T=140°C; 16 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 52, # 19 p. 4381 - 4384
反应条件
nitric acid; hydrazine T=25°C; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 94 - 99
反应条件
in dichloromethane T=25°C; 8 h; Irradiation;
参考文献
Sankararaman,S.; Haney,W.A.; Kochi,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 7824
反应条件
potassium carbonate in acetone 5 h; Heating;
参考文献
Journal of medicinal chemistry, , vol. 38, # 13 p. 2331 - 2338
反应条件
1: 83 percent / aluminium chloride / benzene / 0.5 h / Heating 2: 34 percent / nitric acid, acetic acid / 4 h / 15 - 16 °C / further nitration agents 3: 97 percent / potassium carbonate / dimethylformamide / 14 h / Ambient temperature 4: 8 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
反应条件
1: 34 percent / nitric acid, acetic acid / 4 h / 15 - 16 °C / further nitration agents 2: 97 percent / potassium carbonate / dimethylformamide / 14 h / Ambient temperature 3: 8 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
