3-甲基-4-硝基苯甲醚合成路线 (共 58 条)
反应条件
1: 77 percent / bromine, aluminium powder 2: 83 percent / aluminium chloride / benzene / 0.5 h / Heating 3: 34 percent / nitric acid, acetic acid / 4 h / 15 - 16 °C / further nitration agents 4: 97 percent / potassium carbonate / dimethylformamide / 14 h / Ambient temperature 5: 8 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
反应条件
nitric acid; acetic acid T=5 - 10°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 513, p. 1,18
反应条件
1: 97 percent / potassium carbonate / dimethylformamide / 14 h / Ambient temperature 2: 8 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
反应条件
potassium carbonate; copper(II) oxide T=140°C; 16 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
参考文献
Chemische Berichte, , vol. 31, p. 394
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Journal of Organic Chemistry, , vol. 44, # 13 p. 2087 - 2092
反应条件
potassium permanganate 1.) tetrahydrofuran, 0 deg C, 2.) acetone-water (1:1), 0 deg C.; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 45, # 3 p. 522 - 524
反应条件
1: 16 percent / copper(II) nitrate trihydrate, acetic anhydride / 1.5 h / 30 °C 2: 8 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
参考文献
Helvetica Chimica Acta, , vol. 7, p. 698
反应条件
sulfuric acid anschliessendes Behandeln mit Wasser;
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 4, p. 439