2-氯-1-(2-甲氧基苯基)-乙酮合成路线 （共 9 条）
反应条件
bei der Kalischmelze;
参考文献
Tutin
Journal of the Chemical Society, 1910 , vol. 97, p. 2520
反应条件
[2,2']bipyridinyl; copper(l) chloride in 1,2-dichloro-ethane
3 h; Heating;
参考文献
Ram, Ram N.; Manoj
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5633 - 5635
反应条件
P2O5/silica gel in 1,2-dichloro-ethane
Friedel Crafts acylation; 3 h; Reflux;
参考文献
Zarei, Amin; Hajipour, Abdol R.; Khazdooz, Leila
Tetrahedron Letters, 2008 , vol. 49, # 47 p. 6715 - 6719
反应条件
1: 48 percent / DME / diethyl ether / 0.25 h / -60 °C
2: 76 percent / HCl; EtOH / 1,2-dichloro-ethane / 20 °C
View Scheme
参考文献
Yoshimatsu, Mitsuhiro; Sakai, Miho; Moriura, Eri
European Journal of Organic Chemistry, 2007 , # 3 p. 498 - 507
反应条件
1: 0.2M ammonium nitrate / methanol; H2O / cathodic reduction
2: 5M KOH / ethanol / Heating
3: cond. H2SO4 / H2O; dioxane / 3 h / Ambient temperature
View Scheme
参考文献
Shono, Tatsuya; Kise, Naoki; Yamazaki, Akira; Ohmizu, Hiroshi
Tetrahedron Letters, 1982 , vol. 23, # 15 p. 1609 - 1612
反应条件
1: 5M KOH / ethanol / Heating
2: cond. H2SO4 / H2O; dioxane / 3 h / Ambient temperature
View Scheme
参考文献
Shono, Tatsuya; Kise, Naoki; Yamazaki, Akira; Ohmizu, Hiroshi
Tetrahedron Letters, 1982 , vol. 23, # 15 p. 1609 - 1612
反应条件
1: 91 percent / CHCl3; dimethylformamide / cathodic reduction
2: 90 percent / NaH / tetrahydrofuran / 1 h / 0 °C
3: 0.2M ammonium nitrate / methanol; H2O / cathodic reduction
4: 5M KOH / ethanol / Heating
5: cond. H2SO4 / H2O; dioxane / 3 h / Ambient temperature
View Scheme
参考文献
Shono, Tatsuya; Kise, Naoki; Yamazaki, Akira; Ohmizu, Hiroshi
Tetrahedron Letters, 1982 , vol. 23, # 15 p. 1609 - 1612
反应条件
carbon disulfide; aluminium trichloride
in der Kaelte;
参考文献
Joerlander
Chemische Berichte, 1917 , vol. 50, p. 417
Full Text Show Details
Tutin
Journal of the Chemical Society, 1910 , vol. 97, p. 2520
反应条件
perchloric acid; trichloroisocyanuric acid in acetic acid
T=35°C; effects of varying <TCICA> and <HClO4> on reaction rate; Ea, ΔH(excit.), lgA, ΔS(excit.); KineticsMechanismThermodynamic data;
参考文献
Radhakrishnamurti, P. S.; Rath, Nabeen Kumar
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1985 , vol. 24, # 4 p. 300 - 303
