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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
53689-84-2
合成路线
（共 53 条）
90-90-4
4-溴苯甲酰苯
→
反应条件
53689-84-2
反应条件
1: 1,3-bis(diphenylphosphino)propane; K2CO3 / Pd(OAc)2 / H2O / 1.33 h / 90 °C 2: hydrochloric acid / H2O; ethyl acetate / 20 °C View Scheme
参考文献
Arvela, Riina K.; Pasquini, Serena; Larhed, Mats
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6390 - 6396
6136-66-9
4-碘二苯酮
→
反应条件
53689-84-2
反应条件
1: 1,3-bis(diphenylphosphino)propane; K2CO3 / Pd(OAc)2 / H2O / 1.33 h / 90 °C 2: hydrochloric acid / H2O; ethyl acetate / 20 °C View Scheme
参考文献
Arvela, Riina K.; Pasquini, Serena; Larhed, Mats
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6390 - 6396
99-90-1
4-溴苯乙酮
+
98-80-6
苯硼酸
→
反应条件
92-91-1
联苯单乙酮
+
53689-84-2
反应条件
bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; potassium carbonate in various solvent(s) T=80°C; 16 h; further reagents;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
13329-40-3
4-碘代苯乙酮
+
98-80-6
苯硼酸
→
反应条件
92-91-1
联苯单乙酮
+
53689-84-2
反应条件
bis-triphenylphosphine-palladium(II) chloride; Ti2CO3; carbon monoxide in various solvent(s) T=80°C; 5 h; further reagents and solvents;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
109613-00-5
4-乙酰苯基三氟甲烷磺酸酯
+
98-80-6
苯硼酸
→
反应条件
92-91-1
联苯单乙酮
+
53689-84-2
反应条件
bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; potassium carbonate in various solvent(s) T=80°C; 16 h; further reagents;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
65189-90-4
→
反应条件
1002104-40-6
+
782-92-3
4-(乙酰苯基)苯甲烷
+
53689-84-2
+
85696-44-2
反应条件
oxygen; WOx/SiO2-5.3 in acetonitrile T=5 - 10°C; 1 h; UV-irradiation; Title compound not separated from byproducts.;
参考文献
Tzirakis, Manolis D.; Lykakis, Ioannis N.; Panagiotou, George D.; Bourikas, Kyriakos; Lycourghiotis, Alexis; Kordulis, Christos; Orfanopoulos, Michael
Journal of Catalysis, 2007 , vol. 252, # 2 p. 178 - 189
22543-70-0
→
反应条件
1002104-41-7
+
18220-90-1
4-乙基苯甲酮
+
53689-84-2
+
94705-09-6
反应条件
oxygen; WOx/SiO2-5.3 in acetonitrile T=5 - 10°C; 1 h; UV-irradiation; Title compound not separated from byproducts.;
参考文献
Tzirakis, Manolis D.; Lykakis, Ioannis N.; Panagiotou, George D.; Bourikas, Kyriakos; Lycourghiotis, Alexis; Kordulis, Christos; Orfanopoulos, Michael
Journal of Catalysis, 2007 , vol. 252, # 2 p. 178 - 189
13329-40-3
4-碘代苯乙酮
+
82102-37-2
+
98-80-6
苯硼酸
→
反应条件
92-91-1
联苯单乙酮
+
53689-84-2
反应条件
1: COgen With N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 T=80°C; 2: 4'-iodoacetophenone; 3,4,5-trimethoxyphenylboronic acid With potassium carbonate; palladium dichloride T=80°C; Reagent/catalyst;
参考文献
Ahlburg, Andreas; Lindhardt, Anders T.; Taaning, Rolf. H.; Modvig, Amalie E.; Skrydstrup, Troels
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10310 - 10318
13329-40-3
4-碘代苯乙酮
+
201230-82-2
+
98-80-6
苯硼酸
→
反应条件
92-91-1
联苯单乙酮
+
53689-84-2
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in various solvent(s) T=80°C; P=760 Torr; 5 h; further reagents and solvents;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
1137-42-4
4-羟基-二苯甲酮
→
反应条件
53689-84-2
反应条件
1: K2CO3 / acetone 2: 330 - 470 °C View Scheme
参考文献
Royer,R. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 4308 - 4311
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