phosphorus; hydrogen iodide

1: aq. NaOH 2: phosphorus, HI View Scheme

sodium hydroxide

platinum Hydrogenation;

hydrogenchloride T=110°C; 24 h; structure determination;

hydrogenchloride T=110°C; 24 h; structure determination;

暂无反应条件数据

9H-fluorene T=250°C;

1: Br2 / methanol / Ambient temperature 2: conc. H2SO4 / 46 h / Heating 3: 76 percent / N,N-dicyclohexylcarbodiimide / dioxane / 20 h / Ambient temperature 4: 5.2 percent / thallium(III) trinitrate / 18 h / 4 °C 5: 38 percent / 90percent aq. AcOH, Zn / 1 h / Ambient temperature 6: 78.4 percent / diethyl ether; methanol / 1 h / Ambient temperature 7: 71.4 percent / AcOK, H2 / 5percent Pd/C / methanol / Ambient temperature 8: 63 percent / N,N-dicyclohexylcarbodimide / dioxane / 4 h / Ambient temperature 9: 24 percent / 1N aq. NaOH / methanol; acetonitrile / 0.5 h / Ambient temperature 10: 6.1 mg / H2 / 5percent Pd/C / methanol / 3 h / Ambient temperature 11: 39 percent / N,N-dicyclohexylcarbodimide / dioxane / 15 h 12: 60 percent / AlCl3 / CH2Cl2 / 2 h / Ambient temperature View Scheme

1: Br2 / methanol / Ambient temperature 2: conc. H2SO4 / 46 h / Heating 3: 76 percent / N,N-dicyclohexylcarbodiimide / dioxane / 20 h / Ambient temperature 4: 5.2 percent / thallium(III) trinitrate / 18 h / 4 °C 5: 38 percent / 90percent aq. AcOH, Zn / 1 h / Ambient temperature 6: 78.4 percent / diethyl ether; methanol / 1 h / Ambient temperature 7: 71.4 percent / AcOK, H2 / 5percent Pd/C / methanol / Ambient temperature 8: 63 percent / N,N-dicyclohexylcarbodimide / dioxane / 4 h / Ambient temperature 9: 24 percent / 1N aq. NaOH / methanol; acetonitrile / 0.5 h / Ambient temperature 10: 6.1 mg / H2 / 5percent Pd/C / methanol / 3 h / Ambient temperature 11: 39 percent / N,N-dicyclohexylcarbodimide / dioxane / 15 h View Scheme