1-甲基-3-苯基嘧啶-2,4,6-三酮合成路线 (共 6 条)
参考文献
Krasnov; Slesarev
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 4 p. 543 - 548
参考文献
Nightingale; Taylor
Journal of the American Chemical Society, 1939 , vol. 61, p. 1015
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Hepner; Frenkenberg
Chemische Berichte, 1932 , vol. 65, p. 123,126
反应条件
1: 2N NaOH
2: c-HCl / acetic acid / 80 °C
View Scheme
参考文献
Tobe, Masanori; Isobe, Yoshiaki; Goto, Yuso; Obara, Fumihiro; Tsuchiya, Masami; Matsui, Junko; Hirota, Kosaku; Hayashi, Hideya
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 8 p. 2037 - 2047
反应条件
1: Ac2O / acetic acid / 80 °C
2: 2N NaOH
3: c-HCl / acetic acid / 80 °C
View Scheme
参考文献
Tobe, Masanori; Isobe, Yoshiaki; Goto, Yuso; Obara, Fumihiro; Tsuchiya, Masami; Matsui, Junko; Hirota, Kosaku; Hayashi, Hideya
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 8 p. 2037 - 2047
反应条件
hydrogenchloride; sulfuric acid
参考文献
Hepner; Frenkenberg
Helvetica Chimica Acta, 1932 , vol. 15, p. 350,352
反应条件
trichlorophosphate
T=80°C; Chlorination;
参考文献
Isobe, Yoshiaki; Hirota, Kosaku
Chemical and Pharmaceutical Bulletin, 2003 , vol. 51, # 12 p. 1451 - 1454