(S)-(+)-1,2,3,4-四氢-1-萘酚合成路线 （共 60 条）
反应条件
potassium carbonate in methanol Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 598 - 600
反应条件
2: K2CO3 / methanol / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 598 - 600
反应条件
sodium hydroxide Hydrolysis;
参考文献
Journal of Organic Chemistry, , vol. 64, # 26 p. 9365 - 9373
反应条件
lipase Amano PS30 in various solvent(s) Enzymatic reaction;
参考文献
Merlic; Walsh
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2265 - 2274
反应条件
in hexane Acylation; isobutylation; 18 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 64, # 26 p. 9365 - 9373
反应条件
in benzene T=35°C; 2.5 h; Irradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Tetrahedron Letters, , vol. 39, # 24 p. 4333 - 4336
反应条件
in benzene 2.5 h; HeatingIrradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Tetrahedron Letters, , vol. 39, # 24 p. 4333 - 4336
反应条件
rabbit 3-hydroxyhexobarbital dehydrogenase (AKR1C29); NADP in aq. phosphate buffer; ethyl acetate T=37°C; pH=7.4; 0.5 h; Enzymatic reaction; Catalytic behaviorKinetics;
参考文献
Endo, Satoshi; Matsunaga, Toshiyuki; Matsumoto, Atsuko; Arai, Yuki; Ohno, Satoshi; El-Kabbani, Ossama; Tajima, Kazuo; Bunai, Yasuo; Yamano, Shigeru; Hara, Akira; Kitade, Yukio
Biochemical Pharmacology, 2013 , vol. 86, # 9 p. 1366 - 1375
反应条件
1: rabbit 3-hydroxyhexobarbital dehydrogenase (AKR1C29); NADP / aq. phosphate buffer; ethyl acetate / 0.5 h / 37 °C / pH 7.4 / |Enzymatic reaction 2: rabbit 3-hydroxyhexobarbital dehydrogenase (AKR1C29); NADPH / aq. phosphate buffer; ethyl acetate / 0.5 h / 37 °C / pH 7.4 / |Enzymatic reaction View Scheme
参考文献
Endo, Satoshi; Matsunaga, Toshiyuki; Matsumoto, Atsuko; Arai, Yuki; Ohno, Satoshi; El-Kabbani, Ossama; Tajima, Kazuo; Bunai, Yasuo; Yamano, Shigeru; Hara, Akira; Kitade, Yukio
Biochemical Pharmacology, 2013 , vol. 86, # 9 p. 1366 - 1375
反应条件
1: With diphenylphosphoranyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=0 - 20°C; Azidation; 18 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran Reduction; 2 h; 3: With sodium hydroxide Hydrolysis; Further stages.;
参考文献
Journal of Medicinal Chemistry, , vol. 43, # 7 p. 1329 - 1338
