[4-(1-羟基乙基)苯基]乙酸酯合成路线 （共 12 条）
反应条件
potassium hydrogensulfate T=175 - 200°C;
参考文献
Emerson et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1665
反应条件
aluminum oxide; acetic acid T=350°C; P=25 Torr;
参考文献
Corson et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 544,546
反应条件
1: Ac2O / dimethylformamide / 50 °C 2: KOH / methanol / 20 °C View Scheme
参考文献
Corson et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 544,546
反应条件
sodium tetrahydroborate in isopropyl alcohol
T=0°C; 2.5 h;
参考文献
Noji, Masahiro; Ohno, Tomoko; Fuji, Koji; Futaba, Noriko; Tajima, Hiroyuki; Ishii, Keitaro
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9340 - 9347
反应条件
acetic anhydride in palladium monocarbide
参考文献
HOECHST CELANESE CORPORATION
Patent: EP356070 A1, 1990 ;
反应条件
sodium hydroxide in water; isopropyl alcohol
0.5 h; Ambient temperature;
参考文献
Srivastava; Tandon; Ray
Synthetic Communications, 1992 , vol. 22, # 18 p. 2703 - 2710
反应条件
1: 98 percent / Et3N; 4-dimethylaminopyridine / CH2Cl2 / 0 - 20 °C
2: 91 percent / NaBH4 / propan-2-ol / 2.5 h / 0 °C
View Scheme
参考文献
Noji, Masahiro; Ohno, Tomoko; Fuji, Koji; Futaba, Noriko; Tajima, Hiroyuki; Ishii, Keitaro
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9340 - 9347
反应条件
zinc in N,N-dimethyl-formamide
T=50°C;
参考文献
Kato, Tadahiro; Saito, Naoko; Kashimura, Kaori; Shinohara, Mariko; Kurahashi, Takuma; Taniguchi, Kohji
Journal of Agricultural and Food Chemistry, 2002 , vol. 50, # 22 p. 6307 - 6312
反应条件
1: sodium acetate
2: oxygen; chromium oxide-cobalt hydroxide(?)-calcium carbonate catalyst / 145 °C
3: copper oxide-chromium oxide / 130 °C / 102971 Torr / Hydrogenation
View Scheme
参考文献
Emerson et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1665
反应条件
1: oxygen; chromium oxide-cobalt hydroxide(?)-calcium carbonate catalyst / 145 °C
2: copper oxide-chromium oxide / 130 °C / 102971 Torr / Hydrogenation
View Scheme
参考文献
Emerson et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1665
