1-苯并噻吩-5-基异氰酸酯合成路线 (共 15 条)
参考文献
Jones
Journal of the American Chemical Society, 1949 , vol. 71, p. 383,384
反应条件
potassium permanganate
参考文献
Jones
Journal of the American Chemical Society, 1949 , vol. 71, p. 383,384
反应条件
1: 95 percent / SOCl2 / CHCl3 / 2 h / Heating
2: 97 percent / dimethylformamide / 1 h / 80 °C
3: 85 percent / aq. NaOH / 1.17 h / Heating
4: 44 percent / ethanol / 4.5 h / Heating
View Scheme
参考文献
Birker, Paul J. M. W. L.; Godefroi, Eric F.; Helder, Janneke; Reedijk, Jan
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7556 - 7560
参考文献
Merck and Co., Inc.
Patent: US4746669 A1, 1988 ;
反应条件
hydrogenchloride in dichloromethane
参考文献
Galons, Herve; Bergerat, Isabelle; Combet Farnoux, Claude; Miocque, Marcel
Synthesis, 1982 , # 12 p. 1103 - 1105