2-(2-甲基苯基)-1H-吲哚合成路线 （共 19 条）
反应条件
oxygen; acetic acid; palladium diacetate
T=20°C; P=760.051 Torr; 10 h;
参考文献
Yang, Shang-Dong; Sun, Chang-Liang; Fang, Zhao; Li, Bi-Jie; Li, Yi-Zhou; Shi, Zhang-Jie
Angewandte Chemie - International Edition, 2008 , vol. 47, # 8 p. 1473 - 1476
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium phosphate in toluene
T=90°C; Suzuki-Miyaura coupling; 4 h;
参考文献
Fang, Yuan-Qing; Lautens, Mark
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 538 - 549
反应条件
palladium diacetate; magnesium oxide; triphenylphosphine in 1,4-dioxane; N,N-dimethyl-formamide
T=150°C; 18 h;
参考文献
Lane, Benjamin S.; Brown, Meghann A.; Sames, Dalibor
Journal of the American Chemical Society, 2005 , vol. 127, # 22 p. 8050 - 8057
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine in N,N-dimethyl acetamide
T=20°C; Sonogashira Cross-Coupling; 1 h;
2: With sodium hydroxide in N,N-dimethyl acetamide
T=140°C;
参考文献
Yu, Xufen; Park, Eun-Jung; Kondratyuk, Tamara P.; Pezzuto, John M.; Sun, Dianqing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 44 p. 8835 - 8847
反应条件
sulfuric acid; silver(I) acetate; palladium dichloride in N,N-dimethyl-formamide; acetonitrile
T=100°C; 0.666667 h; Sealed tubeMicrowave irradiation; regioselective reaction;
参考文献
Miao, Tao; Li, Pinhua; Wang, Guan-Wu; Wang, Lei
Chemistry - An Asian Journal, 2013 , vol. 8, # 12 p. 3185 - 3190
反应条件
potassium carbonate in methanol
参考文献
Leboho, Tlabo C.; Michael, Joseph P.; van Otterlo, Willem A.L.; van Vuuren, Sandy F.; de Koning, Charles B.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 17 p. 4948 - 4951
反应条件
C40H50Cl2Ir2N4(2+)*2F6P(1-) in acetonitrile
24 h; Inert atmosphereReflux;
参考文献
Ogata, Kenichi; Nagaya, Toshinori; Fukuzawa, Shin-Ichi
Journal of Organometallic Chemistry, 2010 , vol. 695, # 12-13 p. 1675 - 1681
反应条件
sodium carbonate; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; water
T=20°C; Suzuki-Miyaura cross-coupling; 18 h; Inert atmosphere;
参考文献
Robbins, Daniel W.; Hartwig, John F.
Organic Letters, 2012 , vol. 14, # 16 p. 4266 - 4269
反应条件
1: With palladium diacetate; dimethyl sulfoxide; trifluoroacetic acid
T=90°C; 24 h;
2: With iron
T=90°C; 2 h;
参考文献
Jadhav, Jagannath; Gaikwad, Vipul; Kurane, Rajanikant; Salunkhe, Rajashri; Rashinkar, Gajanan
Synlett, 2012 , vol. 23, # 17 p. 2511 - 2515,5
Title/Abstract Full Text Show Details
Jadhav, Jagannath; Gaikwad, Vipul; Kurane, Rajanikant; Salunkhe, Rajashri; Rashinkar, Gajanan
Synlett, 2012 , vol. 23, # 17 p. 2511 - 2515
反应条件
carbon monoxide; sulfur; triethylamine in N,N-dimethyl-formamide
T=150°C; P=22801.5 Torr; 24 h; Autoclave;
参考文献
Umeda, Rui; Nishimoto, Yuuta; Mashino, Tsukasa; Nishiyama, Yutaka
Heterocycles, 2013 , vol. 87, # 6 p. 1241 - 1247
