N,N-二甲基-1H-吲哚-1-甲胺合成路线 （共 9 条）
反应条件
1: 1.) butyllithium 2: 56 percent / sodium borohydride / ethanol; tetrahydrofuran / Heating View Scheme
参考文献
Katritzky, Alan R.; Lue, Ping; Chen, Ya-Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3688 - 3691
反应条件
1: 1.) butyllithium 2: 71 percent / sodium borohydride / ethanol; tetrahydrofuran / Heating View Scheme
参考文献
Katritzky, Alan R.; Lue, Ping; Chen, Ya-Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3688 - 3691
反应条件
in water
T=0°C; Mannich Reaction;
参考文献
UNIVERSITE JOSEPH FOURIER; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
Patent: US2010/144726 A1, 2010 ;
Location in patent: Page/Page column 44 ;
反应条件
succinic acid anhydride; potassium carbonate in dichloromethane
T=20°C; 1 h; Title compound not separated from byproducts;
参考文献
Love, Brian E.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 630 - 632
反应条件
potassium tert-butylate in tetrahydrofuran
2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Love, Brian E.; Nguyen, Binh T.
Synlett, 1998 , # 10 p. 1123 - 1125
反应条件
in water
1.) 3h, 0 deg C, 2.) up to RT;
参考文献
Katritzky, Alan R.; Lue, Ping; Chen, Ya-Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3688 - 3691
反应条件
1: 1.) butyllithium
2: 67 percent / sodium borohydride / ethanol; tetrahydrofuran / Heating
View Scheme
参考文献
Katritzky, Alan R.; Lue, Ping; Chen, Ya-Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3688 - 3691
反应条件
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; zinc(II) chloride
Yield given. Multistep reaction;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Takazawa, Nobuo; Yamanaka, Hiroshi
Heterocycles, 1993 , vol. 36, # 5 p. 941 - 942
反应条件
1: 1.) butyllithium
2: 51 percent / sodium borohydride / ethanol; tetrahydrofuran / Heating
View Scheme
参考文献
Katritzky, Alan R.; Lue, Ping; Chen, Ya-Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3688 - 3691
