1,2-二对甲苯基乙烷合成路线 (共 169 条)
反应条件
{2,6-(Ph2PO)2-C6H3}NiCl; zinc in N,N-dimethyl-formamide T=115°C; 16 h; Inert atmosphere;
参考文献
Chen, Tao; Yang, Limin; Li, Liang; Huang, Kuo-Wei
Tetrahedron, 2012 , vol. 68, # 31 p. 6152 - 6157
反应条件
tetraethylammonium iodide; zinc; NiBr2(PPh3)2 in tetrahydrofuran Ambient temperature1.) 30 min; 2.) 2 h;
参考文献
Albrecht, M.; Blau, O.
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1998 , vol. 340, # 7 p. 683 - 685
反应条件
nickel copper; carbon in ethylene glycol dimethyl ether T=85°C; 20 h;
参考文献
Journal of Organometallic Chemistry, , vol. 342, p. 137 - 142
反应条件
methyl-magnesium iodide; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in benzene T=46°C; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 57, # 7 p. 2178 - 2182
反应条件
mercury(II) oxide in methanol; acetonitrile T=25°C; UV-irradiation;
参考文献
Habibi, Mohammad H.; Farhadi, Saeid
Journal of Chemical Research, 2004 , # 4 p. 296 - 297
反应条件
1: anhydrous 1-octyne With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2: With zinc dibromide in tetrahydrofuran; hexane T=-78 - 0°C; 3: p-methylbenzyl bromide With [Pd{bis[2-(diphenylphosphino)phenyl] ether}Cl2] in tetrahydrofuran; hexane T=23°C; 10 h;
参考文献
Tetrahedron Letters, , vol. 46, # 16 p. 2927 - 2930
反应条件
C29H33Cl2FeN5*C4H8O in tetrahydrofuran; diethyl ether T=20°C; 0.5 h; Inert atmosphereSchlenk technique;
参考文献
Wu, Jianguo; Dai, Wei; Farnaby, Joy H.; Hazari, Nilay; Le Roy, Jennifer J.; Mereacre, Valeriu; Murugesu, Muralee; Powell, Annie K.; Takase, Michael K.
Dalton Transactions, 2013 , vol. 42, # 20 p. 7404 - 7413
反应条件
1,4-dioxane; nickel Hydrogenation;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 72, p. 793,794
参考文献
Chemical Communications, , # 13 p. 1163 - 1164
反应条件
hydrogenchloride in tetrahydrofuran T=-85 - -40°C; Condensation;
参考文献
Harada, Toshiro; Kaneko, Takayuki; Fujiwara, Takayuki; Oku, Akira
Tetrahedron, 1998 , vol. 54, # 32 p. 9317 - 9332