1,2-二对甲苯基乙烷合成路线 (共 169 条)
反应条件
DCN; oxygen 96 h; Irradiation;
参考文献
Canadian Journal of Chemistry, , vol. 62, p. 424 - 436
反应条件
perchloric acid; hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile T=83°C; 0.416667 h; other reaction condition; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 9 p. 1607 - 1613
反应条件
perchloric acid; hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile
T=83°C; 0.416667 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Camaioni, Donald M.; Franz, James A.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1607 - 1613
反应条件
perchloric acid; hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile
T=83°C; 0.416667 h; other reaction condition; MechanismProduct distribution;
参考文献
Camaioni, Donald M.; Franz, James A.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1607 - 1613
反应条件
perchloric acid; hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile
T=83°C; 0.416667 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Camaioni, Donald M.; Franz, James A.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1607 - 1613
反应条件
perchloric acid; hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile
T=83°C; 0.416667 h; other reaction condition; MechanismProduct distribution;
参考文献
Camaioni, Donald M.; Franz, James A.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1607 - 1613
反应条件
1: S2O8(2-), HClO4 / Cu(ClO4)2 / acetonitrile; H2O / 0.42 h / 83 °C
3: Amberlyst-15 strong acid resin / benzene / Heating
4: H2 / 5percent Pd/C
5: S2O8(2-), HClO4 / Cu(ClO4)2 / acetonitrile; H2O / 0.42 h / 83 °C
View Scheme
参考文献
Camaioni, Donald M.; Franz, James A.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1607 - 1613
反应条件
1: 8 percent / AlCl3 / CS2 / 2 h / Ambient temperature
2: 92 percent / 2 h / 900 - 1000 °C / 0.8 - 3 Torr / flash vacuum pyrolysis of dibenzosuberones, regiospecific formation of anthracenes
View Scheme
参考文献
Meyer,H.; Hofmann
Monatshefte fuer Chemie, 1916 , vol. 37, p. 693
Monatshefte fuer Chemie, 1918 , vol. 39, p. 124
反应条件
ammonium acetate; acetic acid in water
T=117°C; 5 h;
参考文献
SHOWA DENKO K.K.
Patent: WO2006/46736 A1, 2006 ;
Location in patent: Page/Page column 54-55 ;