3-苯氧基-1,2-丙二醇合成路线 （共 55 条）
反应条件
ammonium or phosphonium salts; Yield given;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 27, # 5 p. 552
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 27, # 5 p. 692
参考文献
Monatshefte fuer Chemie, , vol. 29, p. 953
反应条件
1: PPh3, diethylazodicarboxylate / benzene / 12 h / Heating 2: 72 h View Scheme
参考文献
Villa; Pallavicini; Romeo; Valoti; Ferri; Iuliano; Brunello
Farmaco, 1995 , vol. 50, # 10 p. 643 - 658
反应条件
1H-imidazole; N-methyl-N-lt;(methylthio)methylenegt;methanaminium iodide in toluene T=85°C; 3 h; Inert atmosphere; chemoselective reaction;
参考文献
Ellwood, Adam R.; Porter, Michael J.
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7982 - 7985
反应条件
triphenylphosphine; diethylazodicarboxylate in benzene 12 h; Heating; Yield given;
参考文献
Kolb, Hartmuth C.; Sharpless, K. Barry
Tetrahedron, 1992 , vol. 48, # 48 p. 10515 - 10530
反应条件
1H-imidazole; N-methyl-N-lt;(methylthio)methylenegt;methanaminium iodide in toluene T=85°C; 3 h; Inert atmosphere; chemoselective reaction;
参考文献
Ellwood, Adam R.; Porter, Michael J.
Journal of Organic Chemistry, 2009 , vol. 74, # 20 p. 7982 - 7985
参考文献
Gamayurova, V. S.; Niyazov, N. A.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 11 p. 2489 - 2493,2210 - 2213
参考文献
Lunsford,C.D. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 1166 - 1171
反应条件
sodium periodate in dichloromethane
0.166667 h;
参考文献
ASTRAZENECA AB; BAYER SCHERING PHARMA AKTIENGESELLSCHAFT
Patent: WO2008/76048 A1, 2008 ;
Location in patent: Example 68 ;
WO 2008/076048 A1
参考文献
Hatch; Nesbitt
Journal of the American Chemical Society, 1945 , vol. 67, p. 40
Full Text Show Details
Speer; Mahler
Journal of the American Chemical Society, 1949 , vol. 71, p. 1133
