3-苯氧基-1,2-丙二醇合成路线 （共 55 条）
反应条件
1,4-dioxane; sodium methylate
T=25 - 50°C;
参考文献
Resinous Prod. and Chem. Co.
Patent: US2401607 , 1944 ;
Full Text Show Details
Resinous Prod. and Chem. Co.
Patent: US2437905 , 1945 ;
反应条件
sodium hydride in tetrahydrofuran
24 h; Heating;
参考文献
Dishong, Dennis M.; Diamond, Craig J.; Cinoman, Michael I.; Gokel, Geoge W.
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 586 - 593
反应条件
1: ethyl bromide With magnesium in diethyl ether
T=80°C;
2: 1-phenoxymethyl-1,2-ethanediol With dilithium tetrachlorocuprate in tetrahydrofuran; diethyl ether
T=-78 - 20°C;
参考文献
Jacobsen, Elisabeth Egholm; Anthonsen, Thorleif
Canadian Journal of Chemistry, 2002 , vol. 80, # 6 p. 577 - 581
反应条件
acetic acid; lithium bromide in tetrahydrofuran
T=20°C; 5 h;
参考文献
Jacobsen, Elisabeth Egholm; Anthonsen, Thorleif
Canadian Journal of Chemistry, 2002 , vol. 80, # 6 p. 577 - 581
反应条件
Montmorillonite K10 clay
T=20°C; 2 h;
参考文献
Shaikh, Nadim S.; Bhor, Santosh S.; Gajare, Anil S.; Deshpande, Vishnu H.; Wakharkar, Radhika D.
Tetrahedron Letters, 2004 , vol. 45, # 28 p. 5395 - 5398
