Gould, Robert O.; Paton, Michael R.; Ross, John F.; Walkinshaw, Malcolm D.; Crosby, John
Journal of Chemical Research, Miniprint, 1986 , # 5 p. 1372 - 1396
carbon monoxide in diethyl ether High Pressure; under dried N2; addn. of N-methylbenzimine at 25°C to a soln. of W-complex (CO-pressure: 50 atm); stirring for 2 d at room temp., then for 1-2 h at 80-100°C; vac.-evapn. until dryness; residue dissolved in petroleum ether/ether; chromy. (silica gel/petroleum ether/ether); recrystn. from petroleum ether; elem. anal.;
参考文献
Kron, Johanna; Schubert, Ulrich
Journal of Organometallic Chemistry, 1989 , vol. 373, p. 203 - 220
boron trifluoride diethyl etherate in dichloromethane
12 h;
参考文献
Banerji, J.; Saha, M.; Chakrabarti, R.; Das, A. K.; Pandit, U. K.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1204 - 1208
