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471-34-1
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戊基苯
合成路线
（共 173 条）
110-53-2
溴代正戊烷
→
反应条件
538-68-1
戊基苯
反应条件
Fe(acac)3; N,N,N',N,-tetramethylethylenediamine; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in tetrahydrofuran T=0°C; 1.33333 h;
参考文献
Cahiez, Gerard; Habiak, Vanessa; Duplais, Christophe; Moyeux, Alban
Angewandte Chemie - International Edition, 2007 , vol. 46, # 23 p. 4364 - 4366
2270-20-4
5-苯基戊酸
→
反应条件
538-68-1
戊基苯
反应条件
triethylsilane; tris(pentafluorophenyl)-borane in dichloromethane T=20°C;
参考文献
Gevorgyan; Rubin; Liu; Yamamoto
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1672 - 1675
370066-06-1
→
反应条件
538-68-1
戊基苯
+
16002-93-0
反式-1-苯基-1-戊烯
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; methyl-ethyl phosphite; tri-iso-propylsilane in 2-cyclohexylethanol T=160°C; 15 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, p. 3174 - 3175
110-53-2
溴代正戊烷
+
100-59-4
苯基氯化镁
→
反应条件
538-68-1
戊基苯
反应条件
palladium diacetate; (1-Ad)2P(O)H in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; Kumada-Corriu coupling; 20 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Schulzke, Carola
Organic Letters, 2010 , vol. 12, # 10 p. 2298 - 2301
583-03-9
苯戊醇
→
反应条件
538-68-1
戊基苯
反应条件
sulfuric acid; nickel in water T=10°C; 2 h;
参考文献
Okimoto, Mitsuhiro; Takahashi, Yukio; Nagata, Yuji; Satoh, Masanori; Sueda, Satoru; Yamashina, Tsunaki
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 7 p. 1405 - 1406
370066-06-1
→
反应条件
538-68-1
戊基苯
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; methyl-ethyl phosphite; tri-iso-propylsilane T=170°C; 15 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Nakamura, Ryo; Kita, Yusuke; Chatani, Naoto
Journal of the American Chemical Society, 2009 , vol. 131, p. 3174 - 3175
13371-17-0
丁基三苯基氯化膦
+
100-51-6
苯甲醇
→
反应条件
538-68-1
戊基苯
反应条件
1: butyl-triphenylphosphonium chloride With n-butyllithium in hexane; toluene T=25°C; 0.5 h; 2: benzyl alcohol With 1,3-bis-(diphenylphosphino)propane; caesium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in hexane; toluene T=150°C; 72 h; 3: With hydrogen; palladium on activated charcoal P=760 Torr; 2 h;
参考文献
Black, Phillip J.; Edwards, Michael G.; Williams, Jonathan M. J.
European Journal of Organic Chemistry, 2006 , # 19 p. 4367 - 4378
124070-43-5
→
反应条件
538-68-1
戊基苯
反应条件
triethylsilane; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=20°C; 48 h;
参考文献
Yang, Bai-Ling; Tian, Shi-Kai
Chemical Communications, 2010 , vol. 46, # 33 p. 6180 - 6182
628-17-1
1-碘戊烷
+
100-58-3
溴化苯基镁
→
反应条件
538-68-1
戊基苯
反应条件
1: phenyl-magnesium bromide With zinc(II) chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 2: With methyl-magnesium chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-amyl iodide With triphenylphosphine; nickel dichloride in tetrahydrofuran T=0 - 20°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Pekel, Oezgen Oemuer; Erdik, Ender
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7087 - 7090
543-59-9
1-氯戊烷
+
100-59-4
苯基氯化镁
→
反应条件
538-68-1
戊基苯
反应条件
p-tert-butyl-p-(2',6'-dimethoxy-biphenyl-2-yl)phosphine chloride; palladium diacetate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; Kumada-Corriu coupling; 20.4667 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Schulzke, Carola
Organic Letters, 2010 , vol. 12, # 10 p. 2298 - 2301
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