反应条件
in methanol
byproducts: N,N'-dicyclohexylurea; a soln. of B-salt and ligand in MeOH was stirred at ambient temp. for 2wk, H2O was added, mixt. extd. with CH2Cl2, dried over MgSO4; solvent was removed by rotary evaporator, dissolved in CH2Cl2, filtered, solvent was removed, vac. sublimed at 100°C;
参考文献
Spielvogel, Bernard F.; Ahmed, Fahim U.; Silvey, Gary L.; Wisian-Neilson, Patty; McPhail, Andrew T.
Inorganic Chemistry, 1984 , vol. 23, p. 4322 - 4324
