反应条件
1: 4-isopropylmethylbenzene With AlCl3, aluminium chloride; BCl3*C9H13N in 1,2-dichloro-benzene T=150°C; 90 h; GloveboxInert atmosphere; 2: 2,3-dimethylbutane-2,3-diol With triethylamine T=0 - 20°C; 1 h; Inert atmosphere; Overall yield = 66 mg; regioselective reaction;
参考文献
Bagutski, Viktor; Del Grosso, Alessandro; Carrillo, Josue Ayuso; Cade, Ian A.; Helm, Matthew D.; Lawson, James R.; Singleton, Paul J.; Solomon, Sophia A.; Marcelli, Tommaso; Ingleson, Michael J.
Journal of the American Chemical Society, 2013 , vol. 135, # 1 p. 474 - 487