反应条件
1: 79.4 percent / AlCl3 / 1,2-dichloro-ethane / 1) addition of AlCl3 at temperature not exceeding 15 deg C 2) 10 deg C, 1 h 3) 20 deg C, 4 h
2: Mg / 1) ether, 0 deg C, 4 h 2) 20 deg C, 3 h
3: K2CO3, H2O / aq. ethanol / 4 h / Heating
View Scheme
参考文献
Kuchar; Brunova; Rejholec; et al.
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 1 p. 122 - 136