1,3-二苯基丙烷-2-醇合成路线 （共 39 条）
反应条件
sodium tetrahydroborate in methanol; water
参考文献
Lloyd, Matthew G.; Taylor, Richard J. K.; Unsworth, William P.
Organic Letters, 2014 , vol. 16, # 10 p. 2772 - 2775
反应条件
sodium acetate; nickel; aniline
T=170°C; P=73550.8 Torr; Hydrogenation.weiteres Reagens: Aethanol;
参考文献
Koelsch
Journal of the American Chemical Society, 1945 , vol. 67, p. 1718
反应条件
pyridine; oxygen; tetra-(n-butyl)ammonium iodide in water; acetonitrile
T=70°C; P=760.051 Torr; 24 h; chemoselective reaction;
参考文献
Su, Yijin; Sun, Xiang; Wu, Guolin; Jiao, Ning
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9808 - 9812
Angew. Chem., 2013 , p. 9990 - 9994
反应条件
Sb(SPh)3 in diethyl ether; dichloromethane
12 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Bridon, Dominique; Zard, Samir Z.
Tetrahedron, 1989 , vol. 45, # 9 p. 2615 - 2626
反应条件
trimethylsilyl trifluoromethanesulfonate; dimethylsulfide borane complex in dichloromethane
参考文献
Bartels, Birgit; Hunter, Roger
Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6756 - 6765
反应条件
1: With copper(l) iodide in diethyl ether
T=-78 - 20°C; Grignard reaction;
2: With sodium perborate in tetrahydrofuran; water
Oxidation;
参考文献
Farthing, Christopher N.; Marsden, Stephen P.
Tetrahedron Letters, 2000 , vol. 41, # 21 p. 4235 - 4238
反应条件
1: H2 / Pd-C / ethanol
2: H2, aq. HCl / Pd-C / ethanol
View Scheme
参考文献
Mitsui,S. et al.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1897 - 1900
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol
参考文献
Mitsui,S. et al.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1897 - 1900
参考文献
Miyake, Hideyoshi; Fujimura, Masahiro; Tsumura, Takatsugu; Sasaki, Mitsuru
Chemistry Letters, 2006 , vol. 35, # 7 p. 778 - 779
反应条件
potassium hydroxide in diethylene glycol dimethyl ether
Heating;
参考文献
Brook,A.G.; Duff,J.M.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 352 - 360
