1,3-二苯基丙烷-2-醇合成路线 （共 39 条）
反应条件
1: cyclohexane / Irradiation
2: aq. KOH / bis-(2-methoxy-ethyl) ether / Heating
View Scheme
参考文献
Brook,A.G.; Duff,J.M.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 352 - 360
反应条件
oxygen; 2-methylpropane-2-thiol; phosphorous acid trimethyl ester
1) toluene, 80 deg C, 60 min; 2) (MeO)3P, room temperature, 120 min; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
反应条件
copper (I) cyanide
1.) a.) THF, cyclohexane, ether, -78 deg C, 5 min, b.) -30 deg C, 5 min, 2.) 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Klunder, Janice M.; Onami, Tetsuo; Sharpless, K. Barry
Journal of Organic Chemistry, 1989 , vol. 54, # 6 p. 1295 - 1304
反应条件
dilithium tetrachlorocuprate
1.) THF, ether -30 deg C, 30 min, 2.) -30 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Klunder, Janice M.; Onami, Tetsuo; Sharpless, K. Barry
Journal of Organic Chemistry, 1989 , vol. 54, # 6 p. 1295 - 1304
参考文献
Tuot; Guyard
Bulletin de la Societe Chimique de France, 1947 , p. 1087,1092
Full Text Show Details
Golowtschansskaja
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 1243,1245
Chem.Abstr., 1947 , p. 3082
反应条件
acridine acid; dimethylsulfide; oxygen
1) toluene, irradiation, 4 h, 2) MeOH, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Okada, Keiji; Okubo, Katsura; Oda, Masaji
Tetrahedron Letters, 1992 , vol. 33, # 1 p. 83 - 84
参考文献
Ivanov; Vasilev
Doklady Bolgarskoi Akademii Nauk, 1956 , vol. 9, # 4 p. 61,63
Chem.Abstr., 1958 , p. 2817
反应条件
dimethylsulfide; oxygen
1) toluene, irradiation, 4 h, 2) MeOH, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Okada, Keiji; Okubo, Katsura; Oda, Masaji
Tetrahedron Letters, 1992 , vol. 33, # 1 p. 83 - 84
反应条件
mercury; zinc in hydrogenchloride
2 h; Heating; Product distribution;
参考文献
Di Vona, Maria Luisa; Rosnati, Vittorio
Tetrahedron, 1993 , vol. 49, # 47 p. 10925 - 10930
反应条件
potassium hydroxide; Ru(CF3CO2)CO(PPh3)2
T=140°C; 80 h; variat. KOH concentration; Equilibrium constant;
参考文献
Graser, Barbara; Strohmeier, Walter; Marcec, Radovan; Steigerwald, Hannelore
Berichte der Bunsen-Gesellschaft, 1981 , vol. 85, # 7 p. 671 - 677
