6-甲基-2(3H)苯并噻唑酮合成路线 (共 7 条)
参考文献
Journal of the Chemical Society, , p. 1755,1760
反应条件
1: With copper(l) iodide; Na2S*9H2O in N,N-dimethyl-formamide
T=80°C; Inert atmosphere;
2: With acetic acid in N,N-dimethyl-formamide
T=130°C; 36 h; Inert atmosphere;
参考文献
Li, Jiaojiao; Zhang, Yihua; Jiang, Yongwen; Ma, Dawei
Tetrahedron Letters, 2012 , vol. 53, # 20 p. 2511 - 2513
反应条件
palladium diacetate; triethylamine; triphenylphosphine in tetrahydrofuran
T=100 - 110°C; P=20686.5 Torr; 60 h; Autoclave;
参考文献
Troisi, Luigino; Granito, Catia; Perrone, Serena; Rosato, Francesca
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4330 - 4332
反应条件
1: With trifluoroacetic acid in ethanol
3 h; Reflux;
2: With water; sodium hydrogencarbonate
参考文献
Murru, Siva; Mondal, Pravat; Yella, Ramesh; Patel, Bhisma K.
European Journal of Organic Chemistry, 2009 , # 31 p. 5406 - 5413
反应条件
K2S; copper(ll) bromide
T=120°C; 15 h;
参考文献
Yang, Yuan; Zhang, Xiaoyun; Zeng, Weilan; Huang, Hui; Liang, Yun
RSC Advances, 2014 , vol. 4, # 12 p. 6090 - 6093
反应条件
in diethyl ether; water
参考文献
ZENECA LIMITED; ZENECA Pharma S.A.
Patent: EP462831 B1, 1996 ;
参考文献
MITSUBISHI CHEMICAL CORPORATION
Patent: EP1043319 A1, 2000 ;