1-(4-氯苯基)-1,4-戊二酮合成路线 （共 37 条）
反应条件
1: 60 percent / aniline hydrobromide / ethanol / 5 h / Heating 2: 44 percent / glacial acetic acid / H2O / Ambient temperature View Scheme
参考文献
Cerreto; Villa; Retico; Scalzo
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 7 p. 701 - 708
反应条件
1: 42 percent / aniline hydrobromide / ethanol / 3 h / Heating 2: 48 percent / glacial acetic acid / H2O / Ambient temperature View Scheme
参考文献
Cerreto; Villa; Retico; Scalzo
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 7 p. 701 - 708
反应条件
1: 62 percent / aniline hydrobromide / ethanol / 3 h / Heating 2: 77 percent / glacial acetic acid / H2O / Ambient temperature View Scheme
参考文献
Cerreto; Villa; Retico; Scalzo
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 7 p. 701 - 708
反应条件
1: H+ 2: H+ View Scheme
参考文献
Cerreto; Villa; Retico; Scalzo
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 7 p. 701 - 708
反应条件
1: 62 percent / aniline hydrobromide / ethanol / 3 h / Heating 2: 43 percent / glacial acetic acid / H2O / Ambient temperature View Scheme
参考文献
Cerreto; Villa; Retico; Scalzo
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 7 p. 701 - 708
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran Decomposition; Heating;
参考文献
Bradley; Williams; Blann, Kevin; Holzapfel, Cedric W.
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2834 - 2836
反应条件
1: With AlCl3, aluminium chloride
T=25 - 30°C; 1.5 - 1.58333 h;
2: With hydrogenchloride in water
T=0°C;
参考文献
LUPIN LTD
Patent: US2005/256128 A1, 2005 ;
Location in patent: Page/Page column 11 ;
反应条件
(n-Bu4N)4W10O32 in acetonitrile
30.2 h; UV-irradiationInert atmosphere;
参考文献
Ravelli, Davide; Zema, Michele; Mella, Mariella; Fagnoni, Maurizio; Albini, Angelo
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4158 - 4164
反应条件
RhH(CO)(triphenylphosphine)3 in methanol
T=80°C; P=15001.2 Torr; 18 h;
参考文献
Chochois, Helene; Sauthier, Mathieu; Maerten, Eddy; Castanet, Yves; Mortreux, Andre
Tetrahedron, 2006 , vol. 62, # 50 p. 11740 - 11746
反应条件
1: diiodomethane With diethylzinc; trifluoroacetic acid in dichloromethane
T=0°C; 0.5 h;
2: 1-(4-chlorophenyl)-1,3-butanedione in dichloromethane
T=20°C; 5 h;
参考文献
Xue, Song; Li, Le-Zhen; Liu, Yong-Kang; Guo, Qing-Xiang
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 215 - 218
