1-(4-氯苯基)-1,4-戊二酮合成路线 （共 37 条）
反应条件
hydrogenchloride in acetic acid
T=100°C; 0.166667 h;
参考文献
Qian, Chang-Yi; Yamada, Takashi; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 5 p. 1371 - 1378
反应条件
in benzene
6 h; Irradiation;
参考文献
Matsumoto; Okubo; Mikami
Journal of the American Chemical Society, 1998 , vol. 120, # 16 p. 4015 - 4016
反应条件
hydrogenchloride in acetic acid
T=80°C; 0.333333 h;
参考文献
Qian, Chang-Yi; Yamada, Takashi; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 5 p. 1371 - 1378
反应条件
RhH(CO)(triphenylphosphine)3 in methanol
T=60°C; P=30002.4 Torr; 18 h;
参考文献
Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre
Chemical Communications, 2004 , # 13 p. 1520 - 1521
反应条件
potassium cyanide in N,N-dimethyl-formamide
0.5 h; Ambient temperature;
参考文献
Miyashita, Akira; Suzuki, Yumiko; Okumura, Yoko; Iwamoto, Ken-Ichi; Higashino, Takeo
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 1 p. 6 - 11
反应条件
potassium cyanide in N,N-dimethyl-formamide
0.5 h; Ambient temperature;
参考文献
Miyashita; Suzuki; Okumura; Higashino
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 1 p. 252 - 254
反应条件
2-(2-hydroxyethyl)-3-methyl-4-benzylthiazolium chloride; triethylamine
T=70°C; 12 h;
参考文献
Roth, B. D.; Ortwine, D. F.; Hoefle, M. L.; Stratton, C. D.; Sliskovic, D. R.; et al.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 21 - 31
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in benzene
T=25°C; 3 h;
参考文献
Yasuda, Makoto; Oh-hata, Tatsuhiro; Shibata, Ikuya; Baba, Akio; Matsuda, Haruo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 7 p. 859 - 866
反应条件
1: 59 percent / DBU / dimethylformamide
2: 98 percent / KCN / dimethylformamide / 0.5 h / Ambient temperature
View Scheme
参考文献
Miyashita, Akira; Suzuki, Yumiko; Okumura, Yoko; Iwamoto, Ken-Ichi; Higashino, Takeo
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 1 p. 6 - 11
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine
T=80°C; P=15001.5 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
Sauthier, Mathieu; Lamotte, Nicolas; Dheur, Julien; Castanet, Yves; Mortreux, Andre
New Journal of Chemistry, 2009 , vol. 33, # 5 p. 969 - 971
