三环[9.2.2.1(4,8)]十六碳-4,6,8(16),11,13,14-六烯合成路线 （共 19 条）
反应条件
tris-(dimethylamino)-phosphine in tetrahydrofuran
Ambient temperatureIrradiation;
参考文献
Higuchi, Hiroyuki; Tani, Keita; Otsubo, Tetsuo; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4027 - 4036
反应条件
tris-(dimethylamino)-phosphine in tetrahydrofuran
20 h; Irradiation;
参考文献
Higuchi, Hiroyuki; Kugimiya, Masao; Otsubo, Tetsuo; Sakata, Yoshiteru; Misumi, Soichi
Tetrahedron Letters, 1983 , vol. 24, # 25 p. 2593 - 2594
反应条件
in benzene
T=20°C; 0.433333 h; Irradiation;
参考文献
Isaji, Hajime; Yasutake, Mikio; Takemura, Hiroyuki; Sako, Katsuya; Tatemitsu, Hitoshi; Inazu, Takahiko; Shinmyozu, Teruo
European Journal of Organic Chemistry, 2001 , # 13 p. 2487 - 2499
反应条件
1: 96 percent / MCPBA / CH2Cl2 / 48 h / Ambient temperature
2: 60 percent / 500 °C / 1 Torr
3: 80 percent / AlCl3-MeNO2 / benzene / 1.5 h / 50 °C
View Scheme
参考文献
Yamato, Takehiko; Matsumoto, Jun-ichi; Tokuhisa, Kiwamu; Tsuji, Katsuya; Suehiro, Kazuaki; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 20 p. 2675 - 2682
反应条件
1: NaBH4 / ethanol; tetrahydrofuran / 13 h / 40 - 50 °C
2: 53 percent / tris(dimethylamino)phosphine / tetrahydrofuran / Ambient temperature; Irradiation
View Scheme
参考文献
Higuchi, Hiroyuki; Tani, Keita; Otsubo, Tetsuo; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4027 - 4036
反应条件
1: NaNO2, conc. aq. HCl / H2O / Ambient temperature
2: 68 percent / KOH, sodium hydrosulfite / H2O; ethanol / Heating
View Scheme
参考文献
Takemura, Hiroyuki; Shinmyozu, Teruo; Inazu, Takahiko
Tetrahedron Letters, 1988 , vol. 29, # 9 p. 1031 - 1032
反应条件
1: NaBH4 / ethanol; tetrahydrofuran / 13 h / 40 - 50 °C
2: 53 percent / tris(dimethylamino)phosphine / tetrahydrofuran / Ambient temperature; Irradiation
View Scheme
参考文献
Higuchi, Hiroyuki; Tani, Keita; Otsubo, Tetsuo; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4027 - 4036
反应条件
1: 60 percent / 500 °C / 1 Torr
2: 80 percent / AlCl3-MeNO2 / benzene / 1.5 h / 50 °C
View Scheme
参考文献
Yamato, Takehiko; Matsumoto, Jun-ichi; Tokuhisa, Kiwamu; Tsuji, Katsuya; Suehiro, Kazuaki; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 20 p. 2675 - 2682
反应条件
triethyl phosphite
Irradiation;
参考文献
Kannen,N. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 3307 - 3313
