(1a,2a,3b,5b,6a,7a)-四环[5.2.1.02,6.03,5]癸烷合成路线 (共 4 条)
反应条件
in acetone
2 h; Irradiation;
参考文献
Paquette, Leo A.; Carr, Richard V. C.; Charumilind, Pana; Blount, John F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4922 - 4926
反应条件
1: 88 percent / ethyl acetate / -35 °C
2: 15.6 percent / hydrazine (97percent), hydrogen peroxide (30percent) / ethanol / 1) 0 deg C, 30 min, 2) room temp.
4: 59 percent / acetone / 2 h / Irradiation
View Scheme
参考文献
Paquette, Leo A.; Carr, Richard V. C.; Charumilind, Pana; Blount, John F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4922 - 4926
反应条件
1: 15.6 percent / hydrazine (97percent), hydrogen peroxide (30percent) / ethanol / 1) 0 deg C, 30 min, 2) room temp.
3: 59 percent / acetone / 2 h / Irradiation
View Scheme
参考文献
Paquette, Leo A.; Carr, Richard V. C.; Charumilind, Pana; Blount, John F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4922 - 4926
反应条件
2: 59 percent / acetone / 2 h / Irradiation
View Scheme
参考文献
Paquette, Leo A.; Carr, Richard V. C.; Charumilind, Pana; Blount, John F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4922 - 4926