5-甲氧基-8-甲基-四氢萘-1-酮合成路线 (共 6 条)
反应条件
methanesulfonic acid; phosphorus pentoxide
参考文献
Garofalo, Albert W.; Litvak, Joane; Wang, Lisa; Dubenko, Larisa G.; Cooper, Raymond; Bierer, Donald E.
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3369 - 3372
反应条件
1: 1.) NaOH / 1.) H2O
2: 1.) t-BuLi / 1.) THF
3: 53 percent / H2 / Pd/C / ethanol; acetic acid / 3102.89 Torr
4: 86 percent / P2O5, MeSO3H
View Scheme
参考文献
Garofalo, Albert W.; Litvak, Joane; Wang, Lisa; Dubenko, Larisa G.; Cooper, Raymond; Bierer, Donald E.
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3369 - 3372
反应条件
1: 1.) t-BuLi / 1.) THF
2: 53 percent / H2 / Pd/C / ethanol; acetic acid / 3102.89 Torr
3: 86 percent / P2O5, MeSO3H
View Scheme
参考文献
Garofalo, Albert W.; Litvak, Joane; Wang, Lisa; Dubenko, Larisa G.; Cooper, Raymond; Bierer, Donald E.
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3369 - 3372
反应条件
1: 53 percent / H2 / Pd/C / ethanol; acetic acid / 3102.89 Torr
2: 86 percent / P2O5, MeSO3H
View Scheme
参考文献
Garofalo, Albert W.; Litvak, Joane; Wang, Lisa; Dubenko, Larisa G.; Cooper, Raymond; Bierer, Donald E.
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3369 - 3372
反应条件
aluminium trichloride
参考文献
Buu-Hoi et al.
Journal of Organic Chemistry, 1950 , vol. 15, p. 950,954
Full Text Show Details
Herran et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 899,902
Full Text Show Details
Cocker et al.
Journal of the Chemical Society, 1952 , p. 73,75
Journal of the Chemical Society, 1953 , p. 2355,2362
反应条件
phosphorus pentoxide; benzene
参考文献
Paranjpe; Phalnikar; Nargund
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1942 , vol. 11/A, p. 120,122