2,3-二氢-2-苯基-1H-异吲哚-1-酮合成路线 (共 52 条)
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide T=50°C; P=750.075 Torr; 48 h; chemoselective reaction;
参考文献
Marosvoelgyi-Hasko, Diana; Takacs, Attila; Riedl, Zsuzsanna; Kollar, Laszlo
Tetrahedron, 2011 , vol. 67, # 5 p. 1036 - 1040
反应条件
hydrogen; platinum in 1,4-dioxane T=80°C; P=750.075 Torr; Sealed tube;
参考文献
Shi, Linyan; Hu, Lei; Wang, Jiaqing; Cao, Xueqin; Gu, Hongwei
Organic Letters, 2012 , vol. 14, # 7 p. 1876 - 1879
反应条件
chloro-trimethyl-silane in N,N-dimethyl-formamide; acetonitrile T=20°C;
参考文献
Wan, Jieping; Wu, Bin; Pan, Yuanjiang
Tetrahedron, 2007 , vol. 63, # 38 p. 9338 - 9344
反应条件
Co-phthalocyanine; (Ph)2SiH2 in ethanol T=70°C; 12 h; chemoselective reaction;
参考文献
Kumar, Vishal; Sharma, Upendra; Singh, Bikram; Kumar, Neeraj
Australian Journal of Chemistry, 2012 , vol. 65, # 12 p. 1594 - 1598
反应条件
sodium ethanolate; C2H5OOCCH2Co(CO)4 in ethanol T=35°C;
参考文献
Foa, M.; Francalanci, F.; Bencini, E.; Gardano, A.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 293 - 304
反应条件
1: 1-(Chloromethyl)-2-iodobenzene With iso-propylmagnesium bromide in tetrahydrofuran T=-30°C; Substitution; 1 h; 2: phenyl isocyanate in tetrahydrofuran T=-20 - 20°C; Grignard reaction; 2 h; Further stages.;
参考文献
Delacroix; Berillon; Cahiez; Knochel
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 8108 - 8110
反应条件
tert-butyl benzene; hydrogen; platinum in 1,4-dioxane T=80°C; P=750.075 Torr; Sealed tube;
参考文献
Organic Letters, , vol. 14, # 7 p. 1876 - 1879
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 25°C; 0.5 h;
参考文献
Ordonez, Mario; Tibhe, Gaurao D.; Zamudio-Medina, Angel; Viveros-Ceballos, Jose Luis
Synthesis, 2012 , vol. 44, # 4 p. 569 - 574
反应条件
1: With isopropylmagnesium chloride in tetrahydrofuran T=50°C; 2: With bis(dimethylamino)phosphorochloridate in tetrahydrofuran T=50°C;
参考文献
Tsuritani, Takayuki; Kii, Satoshi; Akao, Atsushi; Sato, Kimihiko; Nonoyama, Nobuaki; Mase, Toshiaki; Yasuda, Nobuyoshi
Synlett, 2006 , # 5 p. 801 - 803
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; potassium carbonate in N,N-dimethyl acetamide T=120°C; 2 h; Inert atmosphere;
参考文献
Zheng, Yu; Yu, Gongli; Wu, Jinlong; Dai, Wei-Min
Synlett, 2010 , # 7 p. 1075 - 1080