in diethyl ether refluxed under Ar for ca. 7 h; chromy.; first eluent: Fe3(CO)12 (Et2O/C6H6); second eluent: C7H6OFe(CO)3 (CH2Cl2/C6H6); last eluent: C7H6O(Fe(CO)3)2 (ethyl acetate); recrystn. (C6H6); elem. anal.; IR; UV; NMR; mass spectra;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 5 p. 1677 - 1678
Takeshita, Hitoshi; Hatsui, Toshihide; Shimooda, Isao; Mametsuka, Hiroaki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 7 p. 2291 - 2292